[(1R)-1-[[[(acetylamino)methyl]thio]methyl]-2-[[(1S)-1-[(acetyloxy)methyl]-2-phenylethyl]amino]-2-oxoethyl]methylcarbamic acid 1,1-dimethylethyl ester

Base Information

Chemical Name:[(1R)-1-[[[(acetylamino)methyl]thio]methyl]-2-[[(1S)-1-[(acetyloxy)methyl]-2-phenylethyl]amino]-2-oxoethyl]methylcarbamic acid 1,1-dimethylethyl ester
CAS No.:851706-35-9
Molecular Formula:C₂₃H₃₅N₃O₆S
Molecular Weight:481.613
Hs Code.:

[(1R)-1-[[[(acetylamino)methyl]thio]methyl]-2-[[(1S)-1-[(acetyloxy)methyl]-2-phenylethyl]amino]-2-oxoethyl]methylcarbamic acid 1,1-dimethylethyl ester

Synonyms:[(1R)-1-[[[(acetylamino)methyl]thio]methyl]-2-[[(1S)-1-[(acetyloxy)methyl]-2-phenylethyl]amino]-2-oxoethyl]methylcarbamic acid 1,1-dimethylethyl ester

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Chemical Property of [(1R)-1-[[[(acetylamino)methyl]thio]methyl]-2-[[(1S)-1-[(acetyloxy)methyl]-2-phenylethyl]amino]-2-oxoethyl]methylcarbamic acid 1,1-dimethylethyl ester

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Technology Process of [(1R)-1-[[[(acetylamino)methyl]thio]methyl]-2-[[(1S)-1-[(acetyloxy)methyl]-2-phenylethyl]amino]-2-oxoethyl]methylcarbamic acid 1,1-dimethylethyl ester

There total 3 articles about [(1R)-1-[[[(acetylamino)methyl]thio]methyl]-2-[[(1S)-1-[(acetyloxy)methyl]-2-phenylethyl]amino]-2-oxoethyl]methylcarbamic acid 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: Acetic acid (S)-2-amino-3-phenyl-propyl ester; compound with trifluoro-acetic acid

: 270587-80-9
N-BOC-N-Me-L-Cys(Acm)-OH

: 851706-35-9
[(1R)-1-[[[(acetylamino)methyl]thio]methyl]-2-[[(1S)-1-[(acetyloxy)methyl]-2-phenylethyl]amino]-2-oxoethyl]methylcarbamic acid 1,1-dimethylethyl ester

Guidance literature:: With diethyl cyanophosphonate; triethylamine; In N,N-dimethyl-formamide; at 0 - 25 ℃; for 14h;
DOI:10.3987/COM-04-10287

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 851706-35-9
[(1R)-1-[[[(acetylamino)methyl]thio]methyl]-2-[[(1S)-1-[(acetyloxy)methyl]-2-phenylethyl]amino]-2-oxoethyl]methylcarbamic acid 1,1-dimethylethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: aq. NaOH

2: 96 percent / diethyl phosphorocyanidate; triethylamine / dimethylformamide / 14 h / 0 - 25 °C

With sodium hydroxide; diethyl cyanophosphonate; triethylamine; In N,N-dimethyl-formamide;
DOI:10.3987/COM-04-10287

Reference yield:

: 1001852-00-1
H-NMe-Cys(Acm)-OH

: 851706-35-9
[(1R)-1-[[[(acetylamino)methyl]thio]methyl]-2-[[(1S)-1-[(acetyloxy)methyl]-2-phenylethyl]amino]-2-oxoethyl]methylcarbamic acid 1,1-dimethylethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: aq. NaOH

2: 96 percent / diethyl phosphorocyanidate; triethylamine / dimethylformamide / 14 h / 0 - 25 °C

With sodium hydroxide; diethyl cyanophosphonate; triethylamine; In N,N-dimethyl-formamide;
DOI:10.3987/COM-04-10287