1-benzyl-3-(diaminomethylene)-1-methyl guanidine

Base Information

• Chemical Name: 1-benzyl-3-(diaminomethylene)-1-methyl guanidine
• CAS No.: 21256-23-5
• Molecular Formula: C₁₀H₁₅N₅
• Molecular Weight: 205.263
• Mol file: 21256-23-5.mol

Synonyms:1-benzyl-3-(diaminomethylene)-1-methyl guanidine

Chemical Property of 1-benzyl-3-(diaminomethylene)-1-methyl guanidine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 1-benzyl-3-(diaminomethylene)-1-methyl guanidine

There total 2 articles about 1-benzyl-3-(diaminomethylene)-1-methyl guanidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-methylbenzylamine hydrochloride (13426-94-3) + N-Cyanoguanidine (127099-85-8,780722-26-1,461-58-5) → 1-benzyl-3-(diaminomethylene)-1-methyl guanidine (21256-23-5)

Guidance literature:

DOI:10.1021/ja01523a059

Reference yield:

→ 1-benzyl-3-(diaminomethylene)-1-methyl guanidine (21256-23-5)

Guidance literature:

Reference yield: 26.0%

Phthalic acid dibutyl ester (84-74-2) + 1-benzyl-3-(diaminomethylene)-1-methyl guanidine (21256-23-5) → 1-benzyl-2-(1,5-dioxo-2,5-dihydro-1H-benzo[e][1,3]diazepin-3-yl)-1-methylguanidine

Guidance literature:

1-benzyl-3-(diaminomethylene)-1-methyl guanidine; With potassium tert-butylate; In N,N-dimethyl-formamide; for 0.25h; Cooling with ice;

Phthalic acid dibutyl ester; In N,N-dimethyl-formamide; at 20 ℃;

DOI:10.1039/d0nj01229g

upstream raw materials:

N-methylbenzylamine hydrochloride

N-Cyanoguanidine