C₅₀H₉₂O₃

Base Information

Chemical Name:C₅₀H₉₂O₃
CAS No.:1428645-51-5
Molecular Formula:C₅₀H₉₂O₃
Molecular Weight:741.279
Hs Code.:

C<sub>50</sub>H<sub>92</sub>O<sub>3</sub>

Synonyms:C₅₀H₉₂O₃

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Chemical Property of C₅₀H₉₂O₃

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Technology Process of C₅₀H₉₂O₃

There total 23 articles about C₅₀H₉₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: C₅₁H₉₂O₃

: 1428645-51-5
C₅₀H₉₂O₃

Guidance literature:: With platinum on activated charcoal; hydrogen; In methanol; dichloromethane; for 16h; under 760.051 Torr;
DOI:10.1039/c3ob27277j

Reference yield:

: 210631-01-9
[(S)-2,3-Bis-((3R,7R,11S,15S)-3,7,11,15-tetramethyl-heptadec-16-enyloxy)-propoxymethyl]-benzene

: 1428645-51-5
C₅₀H₉₂O₃

Guidance literature:: Multi-step reaction with 2 steps

1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 48 h / Reflux

2: platinum on activated charcoal; hydrogen / methanol; dichloromethane / 16 h / 760.05 Torr

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; platinum on activated charcoal; hydrogen; In methanol; dichloromethane;
DOI:10.1039/c3ob27277j

Reference yield:

: 24034-73-9
Geranylgeraniol

: 1428645-51-5
C₅₀H₉₂O₃

Guidance literature:: Multi-step reaction with 14 steps

1.1: C₅₂H₄₆O₄P₂Ru; hydrogen / methanol / 16 h / 37503.8 Torr / Schlenk technique; Sealed tube

2.1: 1H-imidazole / dichloromethane / 4 h / 0 - 20 °C / Schlenk technique; Inert atmosphere

3.1: N-Bromosuccinimide / tetrahydrofuran; water / 5 h / 0 °C / Schlenk technique; Inert atmosphere

3.2: Schlenk technique; Inert atmosphere

4.1: periodic acid / tetrahydrofuran / 1 h / 0 °C

5.1: tetrahydrofuran / 16 h / Schlenk technique; Inert atmosphere; Reflux

6.1: diisobutylaluminium hydride / dichloromethane / 0.5 h / Schlenk technique; Inert atmosphere

7.1: C₃₇H₄₀NOPRh; hydrogen / dichloromethane / 16 h / 0 °C / 37503.8 Torr / Schlenk technique

8.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / -78 - 60 °C / Schlenk technique; Inert atmosphere

9.1: n-butyllithium / tetrahydrofuran / 0.5 h / -30 °C / Schlenk technique; Inert atmosphere

9.2: 16 h / -50 - 20 °C / Schlenk technique; Inert atmosphere

10.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / Schlenk technique; Inert atmosphere

11.1: triethylamine / dichloromethane / 2 h / 0 °C / Schlenk technique; Inert atmosphere

12.1: sodium hydride / tetrahydrofuran / 0.25 h / Schlenk technique; Inert atmosphere

12.2: 16 h / Schlenk technique; Inert atmosphere

13.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 48 h / Reflux; Schlenk technique; Inert atmosphere

14.1: hydrogen; platinum on activated charcoal / methanol; dichloromethane / 16 h / Schlenk technique

With 1H-imidazole; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; N-Bromosuccinimide; n-butyllithium; oxalyl dichloride; platinum on activated charcoal; tetrabutyl ammonium fluoride; hydrogen; C₅₂H₄₆O₄P₂Ru; C₃₇H₄₀NOPRh; sodium hydride; diisobutylaluminium hydride; dimethyl sulfoxide; periodic acid; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water; 8.1: |Swern Oxidation;
DOI:10.1002/anie.202104759