4,4'-thiodibenzoyl chloride

Base Information

Chemical Name:4,4'-thiodibenzoyl chloride
CAS No.:14387-35-0
Molecular Formula:C₁₄H₈Cl₂O₂S
Molecular Weight:311.188
Hs Code.:

Synonyms:4,4'-thiodibenzoyl chloride

Suppliers and Price of 4,4'-thiodibenzoyl chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,4'-thiodibenzoyl chloride

Chemical Property:

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Technology Process of 4,4'-thiodibenzoyl chloride

There total 4 articles about 4,4'-thiodibenzoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.9%

: 38217-68-4
C₂₀H₁₄O₄S₂

: 14387-35-0
4,4'-thiodibenzoyl chloride

Guidance literature:: With pyridine; thionyl chloride; at 20 ℃; for 15h; Inert atmosphere; Reflux; Darkness;
DOI:10.1016/j.reactfunctpolym.2011.04.008

Reference yield:

: 456-22-4
4-Fluorobenzoic acid

: 14387-35-0
4,4'-thiodibenzoyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: 1-methyl-pyrrolidin-2-one; sodium benzoate; sodium sulfide hydrate; sodium tosylate; sodium hydroxide / toluene / 125 - 130 °C

2: toluene / 8 h / 200 °C / Inert atmosphere

3: pyridine; thionyl chloride / 15 h / 20 °C / Inert atmosphere; Reflux; Darkness

With pyridine; 1-methyl-pyrrolidin-2-one; sodium benzoate; thionyl chloride; sodium sulfide hydrate; sodium tosylate; sodium hydroxide; In toluene;
DOI:10.1016/j.reactfunctpolym.2011.04.008

Reference yield:

: 46836-99-1
bis(4-cyanophenyl)sulfide

: 14387-35-0
4,4'-thiodibenzoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol / Erhitzen des nach dem Behandeln mit kaltem Wasser isolierten Reaktionsprodukts mit aethanol. Kalilauge

2: thionyl chloride

With thionyl chloride; ethanol;