Technology Process of C30H33ClN6O6
There total 9 articles about C30H33ClN6O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium carbonate; potassium bromide;
In
N,N-dimethyl-formamide;
at 85 ℃;
for 4h;
- Guidance literature:
-
With
tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine;
In
N,N-dimethyl-formamide;
at 60 ℃;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: nitric acid; acetic acid; acetic anhydride / 5 h / 0 - 50 °C
2: hydrogen; palladium 10% on activated carbon / ethyl acetate; methanol / 20 °C
3: ammonium acetate / methanol / 5 h / Reflux
4: trichlorophosphate / toluene / Reflux
5: caesium carbonate / tetrahydrofuran / 50 °C
6: toluene / 4 h / 70 °C
7: tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 60 °C
With
palladium 10% on activated carbon; ammonium acetate; hydrogen; nitric acid; acetic anhydride; tetra-(n-butyl)ammonium iodide; caesium carbonate; acetic acid; N-ethyl-N,N-diisopropylamine; trichlorophosphate;
In
tetrahydrofuran; methanol; ethyl acetate; N,N-dimethyl-formamide; toluene;