sodium 2-4-{2-(4'-chloro-2'-methylbiphenyl-4-ylcarbamoyl)-2-[3-(4,4-dimethylcyclohex-1-enyl)phenyl]ethyl}benzoylaminoethane sulfonic acid

Base Information

Chemical Name:sodium 2-4-{2-(4'-chloro-2'-methylbiphenyl-4-ylcarbamoyl)-2-[3-(4,4-dimethylcyclohex-1-enyl)phenyl]ethyl}benzoylaminoethane sulfonic acid
CAS No.:1207989-11-4
Molecular Formula:C₃₉H₄₂ClN₂O₅S*Na
Molecular Weight:709.282
Hs Code.:

Synonyms:sodium 2-4-{2-(4'-chloro-2'-methylbiphenyl-4-ylcarbamoyl)-2-[3-(4,4-dimethylcyclohex-1-enyl)phenyl]ethyl}benzoylaminoethane sulfonic acid

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Chemical Property of sodium 2-4-{2-(4'-chloro-2'-methylbiphenyl-4-ylcarbamoyl)-2-[3-(4,4-dimethylcyclohex-1-enyl)phenyl]ethyl}benzoylaminoethane sulfonic acid

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Technology Process of sodium 2-4-{2-(4'-chloro-2'-methylbiphenyl-4-ylcarbamoyl)-2-[3-(4,4-dimethylcyclohex-1-enyl)phenyl]ethyl}benzoylaminoethane sulfonic acid

There total 12 articles about sodium 2-4-{2-(4'-chloro-2'-methylbiphenyl-4-ylcarbamoyl)-2-[3-(4,4-dimethylcyclohex-1-enyl)phenyl]ethyl}benzoylaminoethane sulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 107-35-7
Tau

: 4-{2-(4'-chloro-2'-methyl-biphenyl-4-ylcarbamoyl)-2-[3-(4,4-dimethyl-cyclohexyl)-phenyl]-ethyl}-benzoic acid

: 1207989-11-4
sodium 2-4-{2-(4'-chloro-2'-methylbiphenyl-4-ylcarbamoyl)-2-[3-(4,4-dimethylcyclohex-1-enyl)phenyl]ethyl}benzoylaminoethane sulfonic acid

Guidance literature:: Tau; 4-{2-(4'-chloro-2'-methyl-biphenyl-4-ylcarbamoyl)-2-[3-(4,4-dimethyl-cyclohexyl)-phenyl]-ethyl}-benzoic acid; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; for 14h;

With sodium hydrogencarbonate; In water; acetonitrile;

Reference yield:

: 107-35-7
Tau

: {4-(4'-chloro-2'-methylbiphenyl-4-ylcarbamoyl)-2-[3-(4,4-dimethylcyclohexyl)phenyl]ethyl}benzoic acid

: 1207989-11-4
sodium 2-4-{2-(4'-chloro-2'-methylbiphenyl-4-ylcarbamoyl)-2-[3-(4,4-dimethylcyclohex-1-enyl)phenyl]ethyl}benzoylaminoethane sulfonic acid

Guidance literature:: Tau; {4-(4'-chloro-2'-methylbiphenyl-4-ylcarbamoyl)-2-[3-(4,4-dimethylcyclohexyl)phenyl]ethyl}benzoic acid; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; for 14h;

With sodium hydrogencarbonate; In MeCN;

Reference yield:

: 1207989-33-0
4-{3-(4-benzyl-2-oxooxazolidin-3-yl)-2-(3-bromophenyl)-3-oxopropyl}benzoic acid tert-butyl ester

: 1207989-11-4
sodium 2-4-{2-(4'-chloro-2'-methylbiphenyl-4-ylcarbamoyl)-2-[3-(4,4-dimethylcyclohex-1-enyl)phenyl]ethyl}benzoylaminoethane sulfonic acid

Guidance literature:: Multi-step reaction with 6 steps

1.1: lithium hydroxide; dihydrogen peroxide / tetrahydrofuran; water / 3 h / 20 °C

2.1: oxalyl dichloride / dichloromethane / 14 h / 20 °C

2.2: 14 h / 0 - 20 °C

3.1: N-ethyl-N,N-diisopropylamine; dichlorobis(tri-O-tolylphosphine)palladium / 1,2-dimethoxyethane / 2 h / 85 °C

4.1: trifluoroacetic acid; hydrogenchloride / water; dichloromethane / 20 °C

5.1: palladium on activated charcoal; hydrogen / ethyl acetate / 4 h / 20 °C / 760.05 Torr

6.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 14 h

With hydrogenchloride; oxalyl dichloride; dichlorobis(tri-O-tolylphosphine)palladium; palladium on activated charcoal; hydrogen; dihydrogen peroxide; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; lithium hydroxide; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide;