5-<1-<(4-chlorophenyl)methyl>-5-fluorobenzimidazol-2-yl>-4,4-dimethylvaleronitrile

Base Information

Chemical Name:5-<1-<(4-chlorophenyl)methyl>-5-fluorobenzimidazol-2-yl>-4,4-dimethylvaleronitrile
CAS No.:147643-86-5
Molecular Formula:C₂₁H₂₁ClFN₃
Molecular Weight:369.869
Hs Code.:

Synonyms:5-<1-<(4-chlorophenyl)methyl>-5-fluorobenzimidazol-2-yl>-4,4-dimethylvaleronitrile

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-<1-<(4-chlorophenyl)methyl>-5-fluorobenzimidazol-2-yl>-4,4-dimethylvaleronitrile

Chemical Property:

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Technology Process of 5-<1-<(4-chlorophenyl)methyl>-5-fluorobenzimidazol-2-yl>-4,4-dimethylvaleronitrile

There total 4 articles about 5-<1-<(4-chlorophenyl)methyl>-5-fluorobenzimidazol-2-yl>-4,4-dimethylvaleronitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 364-74-9
1,4-difluoro-2-nitrobenzene

: 147643-86-5
5-<1-<(4-chlorophenyl)methyl>-5-fluorobenzimidazol-2-yl>-4,4-dimethylvaleronitrile

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / potassium carbonate / tetrahydrofuran / 8 h / Heating

2: 87 percent / H₂ / Raney nickel / tetrahydrofuran / Ambient temperature

3: 1.) acetic acid, 2.) iodine / 1.) EtOH, RT, 4 h, 2.) 1,2-dimethoxyethane, 50 deg C, 16 h

With hydrogen; iodine; potassium carbonate; acetic acid; nickel; In tetrahydrofuran;

Reference yield:

: 104-86-9
4-chlorobenzylamine

: 147643-86-5
5-<1-<(4-chlorophenyl)methyl>-5-fluorobenzimidazol-2-yl>-4,4-dimethylvaleronitrile

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / potassium carbonate / tetrahydrofuran / 8 h / Heating

2: 87 percent / H₂ / Raney nickel / tetrahydrofuran / Ambient temperature

3: 1.) acetic acid, 2.) iodine / 1.) EtOH, RT, 4 h, 2.) 1,2-dimethoxyethane, 50 deg C, 16 h

With hydrogen; iodine; potassium carbonate; acetic acid; nickel; In tetrahydrofuran;

Reference yield:

: 27099-27-0
2-<<(4-chlorophenyl)methyl>amino>-5-fluoronitrobenzene

: 147643-86-5
5-<1-<(4-chlorophenyl)methyl>-5-fluorobenzimidazol-2-yl>-4,4-dimethylvaleronitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / H₂ / Raney nickel / tetrahydrofuran / Ambient temperature

2: 1.) acetic acid, 2.) iodine / 1.) EtOH, RT, 4 h, 2.) 1,2-dimethoxyethane, 50 deg C, 16 h

With hydrogen; iodine; acetic acid; nickel; In tetrahydrofuran;