2-Amino-5-<1-(benzotriazol-1-yl)-2-hydroxy-2,2-diphenylethyl>-3-methylpyridine

Base Information

Chemical Name:2-Amino-5-<1-(benzotriazol-1-yl)-2-hydroxy-2,2-diphenylethyl>-3-methylpyridine
CAS No.:173960-34-4
Molecular Formula:C₂₆H₂₃N₅O
Molecular Weight:421.502
Hs Code.:

Synonyms:2-Amino-5-<1-(benzotriazol-1-yl)-2-hydroxy-2,2-diphenylethyl>-3-methylpyridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Amino-5-<1-(benzotriazol-1-yl)-2-hydroxy-2,2-diphenylethyl>-3-methylpyridine

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Technology Process of 2-Amino-5-<1-(benzotriazol-1-yl)-2-hydroxy-2,2-diphenylethyl>-3-methylpyridine

There total 3 articles about 2-Amino-5-<1-(benzotriazol-1-yl)-2-hydroxy-2,2-diphenylethyl>-3-methylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 119-61-9
benzophenone

: 173960-14-0
2-Amino-5-(benzotriazol-1-ylmethyl)-3-methylpyridine

: 173960-34-4
2-Amino-5-<1-(benzotriazol-1-yl)-2-hydroxy-2,2-diphenylethyl>-3-methylpyridine

Guidance literature:: With n-butyllithium; In tetrahydrofuran; 1.) -78 deg C, 15 min, 2.) -78 deg C, 15 min;

Reference yield:

: 28539-02-8
1-Hydroxymethyl-1H-benzotriazole

: 173960-34-4
2-Amino-5-<1-(benzotriazol-1-yl)-2-hydroxy-2,2-diphenylethyl>-3-methylpyridine

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / toluene-p-sulfonic acid / acetic acid / 72 h / Heating

2: 72 percent / butyl magnesium chloride / tetrahydrofuran / 0.25 h / -78 °C

With butyl magnesium bromide; toluene-4-sulfonic acid; In tetrahydrofuran; acetic acid; 1: Substitution / 2: Grignard reaction;
DOI:10.1002/(SICI)1096-9063(199912)55:12<1203::AID-PS82>3.0.CO;2-9

Reference yield:

: 1603-40-3
3-methylpyridin-2-ylamine

: 173960-34-4
2-Amino-5-<1-(benzotriazol-1-yl)-2-hydroxy-2,2-diphenylethyl>-3-methylpyridine

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / toluene-p-sulfonic acid / acetic acid / 72 h / Heating

2: 72 percent / butyl magnesium chloride / tetrahydrofuran / 0.25 h / -78 °C

With butyl magnesium bromide; toluene-4-sulfonic acid; In tetrahydrofuran; acetic acid; 1: Substitution / 2: Grignard reaction;
DOI:10.1002/(SICI)1096-9063(199912)55:12<1203::AID-PS82>3.0.CO;2-9