O₂N(Cl)C₆H₃C₆H₂(OBn)(OH)SnBu₃

Base Information

• Chemical Name: O₂N(Cl)C₆H₃C₆H₂(OBn)(OH)SnBu₃
• CAS No.: 1017280-59-9
• Molecular Formula: C₃₁H₄₀ClNO₄Sn
• Molecular Weight: 644.826
• Mol file: 1017280-59-9.mol

Synonyms:O₂N(Cl)C₆H₃C₆H₂(OBn)(OH)SnBu₃

Chemical Property of O₂N(Cl)C₆H₃C₆H₂(OBn)(OH)SnBu₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of O₂N(Cl)C₆H₃C₆H₂(OBn)(OH)SnBu₃

There total 2 articles about O₂N(Cl)C₆H₃C₆H₂(OBn)(OH)SnBu₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

TMSOC6H6OBn (947513-67-9) + O2NC6H3ClCCSnBu3 (1017280-52-2) → O2N(Cl)C6H3C6H2(OBn)(OH)SnBu3 (1017280-59-9)

Guidance literature:

With potassium carbonate; In neat (no solvent); reaction of tin compd. and dihydrobenzene deriv. at 130°C for 18h, treatment with K2CO3 in methanol;

DOI:10.1021/ja7113486

Reference yield: 72.0%

→ O2N(Cl)C6H3C6H2(OBn)(OH)SnBu3 (1017280-59-9)

Guidance literature:

Reference yield: 89.0%

O2N(Cl)C6H3C6H2(OBn)(OH)SnBu3 (1017280-59-9) + methyl iodide (74-88-4) → C32H42ClNO4Sn (1017280-65-7)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide;

upstream raw materials:

TMSOC₆H₆OBn

O₂NC₆H₃ClCCSnBu₃

Downstream raw materials:

C₃₂H₄₂ClNO₄Sn

C₂₁H₁₈ClNO₄

C₂₂H₂₁NO₄

C₂₀H₁₅ClINO₄