C₁₇H₂₂N₄O₆

Base Information

Chemical Name:C₁₇H₂₂N₄O₆
CAS No.:1295471-59-8
Molecular Formula:C₁₇H₂₂N₄O₆
Molecular Weight:378.385
Hs Code.:

C<sub>17</sub>H<sub>22</sub>N<sub>4</sub>O<sub>6</sub>

Synonyms:C₁₇H₂₂N₄O₆

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₇H₂₂N₄O₆

Chemical Property:

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Technology Process of C₁₇H₂₂N₄O₆

There total 14 articles about C₁₇H₂₂N₄O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1295471-56-5
C₁₇H₂₀N₄O₅

: 1295471-59-8
C₁₇H₂₂N₄O₆

Guidance literature:: C₁₇H₂₀N₄O₅; With zinc trifluoromethanesulfonate; acetic acid; at 80 ℃; for 48h;

With methanol; potassium carbonate; at 0 - 20 ℃; for 1h;
DOI:10.1002/anie.201008079

Reference yield:

: C₁₉H₂₄N₄O₇

: 1295471-59-8
C₁₇H₂₂N₄O₆

Guidance literature:: With potassium carbonate; In methanol; at 20 ℃;
DOI:10.1021/jo301638z

Reference yield:

: L-threonine

: 1295471-59-8
C₁₇H₂₂N₄O₆

Guidance literature:: Multi-step reaction with 19 steps

1: thionyl chloride / acetonitrile / 0 - 20 °C

2: lithium hexamethyldisilazane / tetrahydrofuran / -78 °C

3: 2,6-dimethylpyridine / dichloromethane / 0 - 20 °C

4: diisobutylaluminium hydride / dichloromethane / -78 °C

5: methylmagnesium bromide / diethyl ether / 0 °C

6: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / -78 °C

7: ozone / dichloromethane / -78 °C

8: N-ethyl-N,N-diisopropylamine; titanium tetrachloride; chloro-trimethyl-silane / dichloromethane / 0 °C

9: trifluoroacetyl chloride; pyridine / dichloromethane / 20 °C

10: dihydrogen peroxide; sodium hydroxide / methanol; dichloromethane / 0 °C

11: cerium(III) chloride heptahydrate; sodium tetrahydroborate / methanol; dichloromethane / 0 °C

12: pyridine / -78 - 0 °C

13: tetrabutylammoniun azide / toluene / 20 °C

14: trifluoroacetic acid / acetonitrile; water / 0 - 20 °C

15: Dess-Martin periodane / dichloromethane / 0 - 20 °C

16: tetrahydrofuran / -78 °C

17: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C

18: zinc trifluoromethanesulfonate; acetic acid / 80 °C

19: potassium carbonate / methanol / 20 °C

With pyridine; 2,6-dimethylpyridine; sodium tetrahydroborate; chloro-trimethyl-silane; thionyl chloride; oxalyl dichloride; cerium(III) chloride heptahydrate; methylmagnesium bromide; tetrabutyl ammonium fluoride; dihydrogen peroxide; tetrabutylammoniun azide; titanium tetrachloride; zinc trifluoromethanesulfonate; diisobutylaluminium hydride; potassium carbonate; Dess-Martin periodane; ozone; acetic acid; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; trifluoroacetyl chloride; sodium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; toluene; acetonitrile;
DOI:10.1021/jo301638z