(E)-2,2'-(4-((2-(hydroxymethyl)-4-nitrophenyl)diazenyl)phenylazanediyl)diethanol

Base Information

• Chemical Name: (E)-2,2'-(4-((2-(hydroxymethyl)-4-nitrophenyl)diazenyl)phenylazanediyl)diethanol
• CAS No.: 1371596-68-7
• Molecular Formula: C₁₇H₂₀N₄O₅
• Molecular Weight: 360.37
• Mol file: 1371596-68-7.mol

Synonyms:(E)-2,2'-(4-((2-(hydroxymethyl)-4-nitrophenyl)diazenyl)phenylazanediyl)diethanol

Chemical Property of (E)-2,2'-(4-((2-(hydroxymethyl)-4-nitrophenyl)diazenyl)phenylazanediyl)diethanol

Chemical Property:

Purity/Quality:

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Technology Process of (E)-2,2'-(4-((2-(hydroxymethyl)-4-nitrophenyl)diazenyl)phenylazanediyl)diethanol

There total 1 articles about (E)-2,2'-(4-((2-(hydroxymethyl)-4-nitrophenyl)diazenyl)phenylazanediyl)diethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

2,2'-(phenylimino)bis[ethanol] (120-07-0) + (2-amino-5-nitrophenyl)methanol (77242-30-9) → (E)-2,2'-(4-((2-(hydroxymethyl)-4-nitrophenyl)diazenyl)phenylazanediyl)diethanol (1371596-68-7)

Guidance literature:

With hydrogenchloride; sodium nitrite; In water; at 5 ℃; for 2h; Cooling with ice;

DOI:10.1166/jnn.2012.5357

Reference yield: 73.0%

3-maleimidopropionic acid + (E)-2,2'-(4-((2-(hydroxymethyl)-4-nitrophenyl)diazenyl)phenylazanediyl)diethanol (1371596-68-7) → C38H35N7O14

Guidance literature:

With dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate; In tetrahydrofuran; at 20 ℃; for 6h; Inert atmosphere;

DOI:10.1166/jnn.2012.5357

upstream raw materials:

2,2'-(phenylimino)bis[ethanol]

(2-amino-5-nitrophenyl)methanol