9-Phenylbicyclo<3.3.1>nonan-9-ol

Base Information

Chemical Name:9-Phenylbicyclo<3.3.1>nonan-9-ol
CAS No.:33832-17-6
Molecular Formula:C₁₅H₂₀O
Molecular Weight:216.323
Hs Code.:

Synonyms:9-Phenylbicyclo<3.3.1>nonan-9-ol

Suppliers and Price of 9-Phenylbicyclo<3.3.1>nonan-9-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9-Phenylbicyclo<3.3.1>nonan-9-ol

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Technology Process of 9-Phenylbicyclo<3.3.1>nonan-9-ol

There total 3 articles about 9-Phenylbicyclo<3.3.1>nonan-9-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 38050-71-4
9-methoxy-9-BBN

: 3141-47-7
(α,α-dichlorobenzyl)lithium

: 33832-17-6
9-Phenylbicyclo<3.3.1>nonan-9-ol

Guidance literature:: With sodium hydroxide; dihydrogen peroxide; In tetrahydrofuran; -100°C, after 15 min warming to room temp. with stirring, keeping overnight, treating with H2O2-NaOH at 0°C, stirring for 1 h at room temp. and for 15 min at 50°C; Aq. phase is satd. with K2CO3, extd. with diethyl ether, combined organic phases are dried (K2CO3), concd., chromd. (silicagel, ethyl acetate-petroleum ether);
DOI:10.1016/0022-328X(89)87060-3