succinic acid mono-4-hydroxy-4-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cis-cyclohexyl ester

Base Information

Chemical Name:succinic acid mono-4-hydroxy-4-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cis-cyclohexyl ester
CAS No.:1224949-15-8
Molecular Formula:C₂₇H₃₀N₂O₆
Molecular Weight:478.545
Hs Code.:

Synonyms:succinic acid mono-4-hydroxy-4-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cis-cyclohexyl ester

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Chemical Property of succinic acid mono-4-hydroxy-4-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cis-cyclohexyl ester

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Technology Process of succinic acid mono-4-hydroxy-4-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cis-cyclohexyl ester

There total 8 articles about succinic acid mono-4-hydroxy-4-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cis-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

: 108-30-5
succinic acid anhydride

: 1224948-06-4
1-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)cyclohexane-cis-1,4-diol

: 1224949-15-8
succinic acid mono-4-hydroxy-4-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cis-cyclohexyl ester

Guidance literature:: 1-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)cyclohexane-cis-1,4-diol; With sodium hydride; In N,N-dimethyl-formamide; for 0.5h;

succinic acid anhydride; In N,N-dimethyl-formamide; for 12h;

Reference yield:

: 1224949-51-2
8-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-1,4-dioxaspiro[4.5]decan-8-ol

: 1224949-15-8
succinic acid mono-4-hydroxy-4-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cis-cyclohexyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride; water / tetrahydrofuran / 15 h / 20 °C

1.2: 0 °C

2.1: sodium tetrahydroborate; methanol / 2 h / 20 °C

3.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h

3.2: 12 h

With hydrogenchloride; methanol; sodium tetrahydroborate; water; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: 1224949-36-3
3-(8-hydroxy-1,4-dioxaspiro[4.5]decan-8-yl)-1-(p-tolyl)-2-propyn-1-one

: 1224949-15-8
succinic acid mono-4-hydroxy-4-(1-(4-methoxyphenyl)-5-(p-tolyl)-1H-pyrazol-3-yl)-cis-cyclohexyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / ethanol / 0.5 h / 20 °C

1.2: 15 h / 20 °C

2.1: hydrogenchloride; water / tetrahydrofuran / 15 h / 20 °C

2.2: 0 °C

3.1: sodium tetrahydroborate; methanol / 2 h / 20 °C

4.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h

4.2: 12 h

With hydrogenchloride; methanol; sodium tetrahydroborate; water; sodium hydride; triethylamine; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;