p-chlorophenyl 2-amino-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:p-chlorophenyl 2-amino-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranoside
CAS No.:1352306-48-9
Molecular Formula:C₁₉H₂₀ClNO₄S
Molecular Weight:393.891
Hs Code.:

Synonyms:p-chlorophenyl 2-amino-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranoside

Suppliers and Price of p-chlorophenyl 2-amino-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-chlorophenyl 2-amino-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranoside

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Technology Process of p-chlorophenyl 2-amino-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranoside

There total 1 articles about p-chlorophenyl 2-amino-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.3%

: 296768-93-9
4-chlorophenyl 4,6-O-benzylidene-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

: 1352306-48-9
p-chlorophenyl 2-amino-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranoside

Guidance literature:: With ethylenediamine; In ethanol; at 95 ℃; Reflux;
DOI:10.1016/j.carres.2011.09.015

Reference yield: 87.7%

: 1352306-48-9
p-chlorophenyl 2-amino-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranoside

: 7693-46-1
4-Nitrophenyl chloroformate

: 1352306-51-4
C₂₀H₁₈ClNO₅S

Guidance literature:: With sodium hydrogencarbonate; In water; acetonitrile; at 0 - 20 ℃;
DOI:10.1016/j.carres.2011.09.015

Reference yield:

: 1352306-48-9
p-chlorophenyl 2-amino-4,6-O-benzylidene-2-deoxy-1-thio-β-D-glucopyranoside

: 1352306-60-5
p-chlorophenyl 2-acetamido-4-O-acetyl-6-O-benzyl-2-deoxy-2,3-N,O-carbonyl-1-thio-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydrogencarbonate / water; acetonitrile / 0 - 20 °C

2: sodium hydride / N,N-dimethyl-formamide / -10 - 20 °C

3: triethylsilane; boron trifluoride diethyl etherate / dichloromethane / 2 h / 0 °C / Inert atmosphere

4: pyridine / dichloromethane / 3.5 h / -10 - 0 °C

5: N,N-dimethyl-formamide / 60 °C

With pyridine; triethylsilane; boron trifluoride diethyl etherate; sodium hydride; sodium hydrogencarbonate; In dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.carres.2011.09.015