(2Z)-4-{[tert-butyl(dimethyl)silyl]oxy}-3-(3,4-difluorophenyl)-2-[4(methylsulfonyl)phenyl]but-2-en-1-yl N-2,N-6-bis(tert-butoxycarbonyl)lysinate

Base Information

Chemical Name:(2Z)-4-{[tert-butyl(dimethyl)silyl]oxy}-3-(3,4-difluorophenyl)-2-[4(methylsulfonyl)phenyl]but-2-en-1-yl N-2,N-6-bis(tert-butoxycarbonyl)lysinate
CAS No.:885020-51-9
Molecular Formula:C₃₉H₅₈F₂N₂O₉SSi
Molecular Weight:797.046
Hs Code.:

Synonyms:(2Z)-4-{[tert-butyl(dimethyl)silyl]oxy}-3-(3,4-difluorophenyl)-2-[4(methylsulfonyl)phenyl]but-2-en-1-yl N-2,N-6-bis(tert-butoxycarbonyl)lysinate

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Chemical Property of (2Z)-4-{[tert-butyl(dimethyl)silyl]oxy}-3-(3,4-difluorophenyl)-2-[4(methylsulfonyl)phenyl]but-2-en-1-yl N-2,N-6-bis(tert-butoxycarbonyl)lysinate

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Technology Process of (2Z)-4-{[tert-butyl(dimethyl)silyl]oxy}-3-(3,4-difluorophenyl)-2-[4(methylsulfonyl)phenyl]but-2-en-1-yl N-2,N-6-bis(tert-butoxycarbonyl)lysinate

There total 1 articles about (2Z)-4-{[tert-butyl(dimethyl)silyl]oxy}-3-(3,4-difluorophenyl)-2-[4(methylsulfonyl)phenyl]but-2-en-1-yl N-2,N-6-bis(tert-butoxycarbonyl)lysinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 885020-48-4
(2Z)-4-{[tert-butyl(dimethyl)silyl]oxy}-3-(3,4-difluorophenyl)-2-[4-(methylsulfonyl)phenyl]but-2-en-1-ol

: 2483-46-7
Boc-Lys(Boc)-OH

: 885020-51-9
(2Z)-4-{[tert-butyl(dimethyl)silyl]oxy}-3-(3,4-difluorophenyl)-2-[4(methylsulfonyl)phenyl]but-2-en-1-yl N-2,N-6-bis(tert-butoxycarbonyl)lysinate

Guidance literature:: Boc-Lys(Boc)-OH; With 4-methyl-morpholine; HATU; In N,N-dimethyl-formamide; for 0.0833333h;

(2Z)-4-{[tert-butyl(dimethyl)silyl]oxy}-3-(3,4-difluorophenyl)-2-[4-(methylsulfonyl)phenyl]but-2-en-1-ol; In N,N-dimethyl-formamide; for 16h;

In water; N,N-dimethyl-formamide; pH=7;

Reference yield:

: 885020-51-9
(2Z)-4-{[tert-butyl(dimethyl)silyl]oxy}-3-(3,4-difluorophenyl)-2-[4(methylsulfonyl)phenyl]but-2-en-1-yl N-2,N-6-bis(tert-butoxycarbonyl)lysinate

: C₃₃H₄₄F₂N₂O₉S

Guidance literature:: (2Z)-4-{[tert-butyl(dimethyl)silyl]oxy}-3-(3,4-difluorophenyl)-2-[4(methylsulfonyl)phenyl]but-2-en-1-yl N-2,N-6-bis(tert-butoxycarbonyl)lysinate; With fluorosilicic acid; water; In acetonitrile; tert-butyl alcohol; for 3h;

In water; acetonitrile; tert-butyl alcohol; pH=7;