4,12-bis(p-tolylsulfonyl)-4,12-diazapentadecane-1,15-diyl bis(methanesulfonate)

Base Information

Chemical Name:4,12-bis(p-tolylsulfonyl)-4,12-diazapentadecane-1,15-diyl bis(methanesulfonate)
CAS No.:81522-66-9
Molecular Formula:C₂₉H₄₆N₂O₁₀S₄
Molecular Weight:710.956
Hs Code.:

Synonyms:4,12-bis(p-tolylsulfonyl)-4,12-diazapentadecane-1,15-diyl bis(methanesulfonate)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,12-bis(p-tolylsulfonyl)-4,12-diazapentadecane-1,15-diyl bis(methanesulfonate)

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Technology Process of 4,12-bis(p-tolylsulfonyl)-4,12-diazapentadecane-1,15-diyl bis(methanesulfonate)

There total 4 articles about 4,12-bis(p-tolylsulfonyl)-4,12-diazapentadecane-1,15-diyl bis(methanesulfonate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 124-63-0
methanesulfonyl chloride

: 81505-99-9
4,12-bis(p-tolylsulfonyl)-4,12-diazapentadecane-1,15-diol

: 81522-66-9
4,12-bis(p-tolylsulfonyl)-4,12-diazapentadecane-1,15-diyl bis(methanesulfonate)

Guidance literature:: With triethylamine; In dichloromethane;
DOI:10.1021/ja00376a056

Reference yield:

: 646-19-5
heptane-1,7-diamine

: 81522-66-9
4,12-bis(p-tolylsulfonyl)-4,12-diazapentadecane-1,15-diyl bis(methanesulfonate)

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / K₂CO₃ / H₂O / 24 h / 80 °C

2: 88 percent / K₂CO₃ / dimethylformamide / 24 h / 80 °C

3: 90 percent / Et₃N / CH₂Cl₂ / 1.) 0 deg C, 90 min, 2.) RT, 3 h

With potassium carbonate; triethylamine; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19860690308

Reference yield:

: 81505-98-8
N¹,N⁷-di(p-toluenesulfonyl)-1,7-diaminoheptane

: 81522-66-9
4,12-bis(p-tolylsulfonyl)-4,12-diazapentadecane-1,15-diyl bis(methanesulfonate)

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / K₂CO₃ / dimethylformamide / 24 h / 80 °C

2: 90 percent / Et₃N / CH₂Cl₂ / 1.) 0 deg C, 90 min, 2.) RT, 3 h

With potassium carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19860690308