allyl (S)-4-(N-benzyl-2-((tert-butoxycarbonyl)amino)-4-methoxy-4-oxobutanamido)-4-(benzylcarbamoyl)piperidine-1-carboxylate

Base Information

Chemical Name:allyl (S)-4-(N-benzyl-2-((tert-butoxycarbonyl)amino)-4-methoxy-4-oxobutanamido)-4-(benzylcarbamoyl)piperidine-1-carboxylate
CAS No.:1621105-16-5
Molecular Formula:C₃₄H₄₄N₄O₈
Molecular Weight:636.745
Hs Code.:

Synonyms:allyl (S)-4-(N-benzyl-2-((tert-butoxycarbonyl)amino)-4-methoxy-4-oxobutanamido)-4-(benzylcarbamoyl)piperidine-1-carboxylate

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Chemical Property of allyl (S)-4-(N-benzyl-2-((tert-butoxycarbonyl)amino)-4-methoxy-4-oxobutanamido)-4-(benzylcarbamoyl)piperidine-1-carboxylate

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Technology Process of allyl (S)-4-(N-benzyl-2-((tert-butoxycarbonyl)amino)-4-methoxy-4-oxobutanamido)-4-(benzylcarbamoyl)piperidine-1-carboxylate

There total 1 articles about allyl (S)-4-(N-benzyl-2-((tert-butoxycarbonyl)amino)-4-methoxy-4-oxobutanamido)-4-(benzylcarbamoyl)piperidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 88333-03-3,10340-91-7
Benzyl isocyanide

: 59768-74-0,124184-67-4
(S)-2-t-butoxycarbonylaminosuccinic acid 4-methyl ester

: 100-46-9
benzylamine

: 306296-67-3
1-allyloxycarbonylpiperidin-4-one

: 1621105-16-5
allyl (S)-4-(N-benzyl-2-((tert-butoxycarbonyl)amino)-4-methoxy-4-oxobutanamido)-4-(benzylcarbamoyl)piperidine-1-carboxylate

Guidance literature:: Benzyl isocyanide; (S)-2-t-butoxycarbonylaminosuccinic acid 4-methyl ester; benzylamine; 1-allyloxycarbonylpiperidin-4-one; In methanol; at 20 ℃; for 96h;

With hydrogenchloride; In methanol; at 20 ℃; for 0.5h;
DOI:10.1016/j.ejmech.2014.06.026

Reference yield: 83.0%

: 1621105-16-5
allyl (S)-4-(N-benzyl-2-((tert-butoxycarbonyl)amino)-4-methoxy-4-oxobutanamido)-4-(benzylcarbamoyl)piperidine-1-carboxylate

: 1621105-54-1
methyl (S)-4-(benzyl(4-(benzylcarbamoyl)piperidin-4-yl)amino)-3-((tert-butoxycarbonyl)amino-4-oxobutanoate)

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; phenylsilane; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1016/j.ejmech.2014.06.026