4-methoxy-N-(3-methoxyphenyl)benzenesulfonamide

Base Information

Chemical Name:4-methoxy-N-(3-methoxyphenyl)benzenesulfonamide
CAS No.:169945-40-8
Molecular Formula:C₁₄H₁₅NO₄S
Molecular Weight:293.343
Hs Code.:
DSSTox Substance ID:DTXSID301242773

Synonyms:4-methoxy-N-(3-methoxyphenyl)benzenesulfonamide;Cambridge id 5350787;Oprea1_281482;Oprea1_604191;SCHEMBL8711296;JUMKJLMWARUBBW-UHFFFAOYSA-N;DTXSID301242773;STK401861;AKOS001445592;Z45630681;169945-40-8

Suppliers and Price of 4-methoxy-N-(3-methoxyphenyl)benzenesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-methoxy-N-(3-methoxyphenyl)benzenesulfonamide

Chemical Property:

XLogP3:2.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:5
Exact Mass:293.07217913
Heavy Atom Count:20
Complexity:385

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=CC=C(C=C1)S(=O)(=O)NC2=CC(=CC=C2)OC

Technology Process of 4-methoxy-N-(3-methoxyphenyl)benzenesulfonamide

There total 4 articles about 4-methoxy-N-(3-methoxyphenyl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.6%

: 536-90-3,918666-97-4
m-Anisidine

: 98-68-0
4-methoxy-phenyl-sulphonyl chloride

: 169945-40-8
4-methoxy-N-(3-methoxyphenyl)benzenesulfonamide

Guidance literature:: m-Anisidine; With pyridine; In dichloromethane; for 0.166667h;

4-methoxy-phenyl-sulphonyl chloride; In dichloromethane; for 0.25h;
DOI:10.1016/j.tetlet.2013.06.024

Reference yield:

: C₁₅H₁₅NO₆S

: 169945-40-8
4-methoxy-N-(3-methoxyphenyl)benzenesulfonamide

Guidance literature:: With palladium diacetate; In 1,2-dichloro-ethane; at 120 ℃; for 12h;
DOI:10.1002/chem.201500331

Reference yield:

: 4547-64-2
4-methoxybenzenesulfonyl azide

: 169945-40-8
4-methoxy-N-(3-methoxyphenyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; silver(I) triflimide; lithium acetate / 1,2-dichloro-ethane / 24 h / 50 °C

2: palladium diacetate / 1,2-dichloro-ethane / 12 h / 120 °C

With bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; lithium acetate; palladium diacetate; silver(I) triflimide; In 1,2-dichloro-ethane;
DOI:10.1002/chem.201500331