2-(6-benzyloxybenzo[d]thiazol-2-yl)-5H-isochromeno[3,4-d]thiazol-5-one

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Chemical Name:2-(6-benzyloxybenzo[d]thiazol-2-yl)-5H-isochromeno[3,4-d]thiazol-5-one
CAS No.:1620833-30-8
Molecular Formula:C₂₄H₁₄N₂O₃S₂
Molecular Weight:442.519
Hs Code.:

Synonyms:2-(6-benzyloxybenzo[d]thiazol-2-yl)-5H-isochromeno[3,4-d]thiazol-5-one

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Chemical Property of 2-(6-benzyloxybenzo[d]thiazol-2-yl)-5H-isochromeno[3,4-d]thiazol-5-one

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Technology Process of 2-(6-benzyloxybenzo[d]thiazol-2-yl)-5H-isochromeno[3,4-d]thiazol-5-one

There total 2 articles about 2-(6-benzyloxybenzo[d]thiazol-2-yl)-5H-isochromeno[3,4-d]thiazol-5-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 1620833-22-8
6-(benzyloxy)benzo[d]thiazole-2-carbothioamide

: 137420-59-8
2-(2-methoxycarbonyl-phenyl)-2-bromo-acetic acid methyl ester

: 1620833-30-8
2-(6-benzyloxybenzo[d]thiazol-2-yl)-5H-isochromeno[3,4-d]thiazol-5-one

Guidance literature:: 6-(benzyloxy)benzo[d]thiazole-2-carbothioamide; With triethylamine; In N,N-dimethyl-formamide; at 30 ℃; for 0.333333h; Inert atmosphere;

2-(2-methoxycarbonyl-phenyl)-2-bromo-acetic acid methyl ester; In N,N-dimethyl-formamide; at 120 ℃; for 24h; Inert atmosphere;
DOI:10.1055/s-0033-1340048

Reference yield:

: 716-43-8
dimethyl homophthalate

: 1620833-30-8
2-(6-benzyloxybenzo[d]thiazol-2-yl)-5H-isochromeno[3,4-d]thiazol-5-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-Bromosuccinimide / dichloromethane / 18 h / Reflux; UV-irradiation

2.1: triethylamine / N,N-dimethyl-formamide / 0.33 h / 30 °C / Inert atmosphere

2.2: 24 h / 120 °C / Inert atmosphere

With N-Bromosuccinimide; triethylamine; In dichloromethane; N,N-dimethyl-formamide; 2.2: |Hantzsch Thiazole Synthesis;
DOI:10.1055/s-0033-1340048