2-<(p-tolylsulfonyl)oxy>ethyl N,N,N',N'-tetraethylphosphorodiamidate

Base Information

Chemical Name:2-<(p-tolylsulfonyl)oxy>ethyl N,N,N',N'-tetraethylphosphorodiamidate
CAS No.:158382-40-2
Molecular Formula:C₁₇H₃₁N₂O₅PS
Molecular Weight:406.483
Hs Code.:

Synonyms:2-<(p-tolylsulfonyl)oxy>ethyl N,N,N',N'-tetraethylphosphorodiamidate

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Chemical Property of 2-<(p-tolylsulfonyl)oxy>ethyl N,N,N',N'-tetraethylphosphorodiamidate

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Technology Process of 2-<(p-tolylsulfonyl)oxy>ethyl N,N,N',N'-tetraethylphosphorodiamidate

There total 3 articles about 2-<(p-tolylsulfonyl)oxy>ethyl N,N,N',N'-tetraethylphosphorodiamidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 98-59-9
p-toluenesulfonyl chloride

: 158382-39-9
2-hydroxyethyl N,N,N',N'-tetraethylphosphorodiamidate

: 158382-40-2
2-<(p-tolylsulfonyl)oxy>ethyl N,N,N',N'-tetraethylphosphorodiamidate

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; water; Ambient temperature;
DOI:10.1021/jm00036a016

Reference yield:

: 1794-24-7
tetraethyldiamidochlorophosphate

: 158382-40-2
2-<(p-tolylsulfonyl)oxy>ethyl N,N,N',N'-tetraethylphosphorodiamidate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaH / 1.) THF, 0 deg C, 2.) THF, RT, 18 h

2: 72 percent / p-toluenesulfonic acid, MeOH / 8 h / Heating

3: 99 percent / NaOH / tetrahydrofuran; H₂O / Ambient temperature

With methanol; sodium hydroxide; sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; water;
DOI:10.1021/jm00036a016

Reference yield:

: 158382-38-8
2-(tetrahydropyranyloxy)ethyl N,N,N',N'-tetraethylphosphorodiamidate

: 158382-40-2
2-<(p-tolylsulfonyl)oxy>ethyl N,N,N',N'-tetraethylphosphorodiamidate

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / p-toluenesulfonic acid, MeOH / 8 h / Heating

2: 99 percent / NaOH / tetrahydrofuran; H₂O / Ambient temperature

With methanol; sodium hydroxide; toluene-4-sulfonic acid; In tetrahydrofuran; water;
DOI:10.1021/jm00036a016