benzyl (6aS)-6a,7,8,9-tetrahydro-6H-azolo[1,2-d]benzo[b][1,4]oxazine-3-carboxylate

Base Information

Chemical Name:benzyl (6aS)-6a,7,8,9-tetrahydro-6H-azolo[1,2-d]benzo[b][1,4]oxazine-3-carboxylate
CAS No.:463361-52-6
Molecular Formula:C₁₉H₂₀N₂O₃
Molecular Weight:324.379
Hs Code.:

Synonyms:benzyl (6aS)-6a,7,8,9-tetrahydro-6H-azolo[1,2-d]benzo[b][1,4]oxazine-3-carboxylate

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Chemical Property of benzyl (6aS)-6a,7,8,9-tetrahydro-6H-azolo[1,2-d]benzo[b][1,4]oxazine-3-carboxylate

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Technology Process of benzyl (6aS)-6a,7,8,9-tetrahydro-6H-azolo[1,2-d]benzo[b][1,4]oxazine-3-carboxylate

There total 4 articles about benzyl (6aS)-6a,7,8,9-tetrahydro-6H-azolo[1,2-d]benzo[b][1,4]oxazine-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 501-53-1,94274-21-2
benzyl chloroformate

: 463361-98-0
2,3,3a,4-tetrahydro-1H-5-oxa-9b-aza-cyclopenta[a]naphthalen-7-ylamine

: 463361-52-6
benzyl (6aS)-6a,7,8,9-tetrahydro-6H-azolo[1,2-d]benzo[b][1,4]oxazine-3-carboxylate

Guidance literature:: With sodium carbonate; In acetone; toluene; at 20 ℃; for 4h;
DOI:10.1021/jm020092y

Reference yield:

: 369-34-6
3,4-difluoronitrobenzene

: 463361-52-6
benzyl (6aS)-6a,7,8,9-tetrahydro-6H-azolo[1,2-d]benzo[b][1,4]oxazine-3-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / aq. KOH / dimethylsulfoxide / 4 h / 60 °C

2: Fe; aq. HCl / ethanol / 1 h / 20 °C

3: 73 percent / aq. Na₂CO₃ / acetone; toluene / 4 h / 20 °C

With hydrogenchloride; potassium hydroxide; iron; sodium carbonate; In ethanol; dimethyl sulfoxide; acetone; toluene;
DOI:10.1021/jm020092y

Reference yield:

: 23356-96-9
(S)-1-Pyrrolidin-2-yl-methanol

: 463361-52-6
benzyl (6aS)-6a,7,8,9-tetrahydro-6H-azolo[1,2-d]benzo[b][1,4]oxazine-3-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / aq. KOH / dimethylsulfoxide / 4 h / 60 °C

2: Fe; aq. HCl / ethanol / 1 h / 20 °C

3: 73 percent / aq. Na₂CO₃ / acetone; toluene / 4 h / 20 °C

With hydrogenchloride; potassium hydroxide; iron; sodium carbonate; In ethanol; dimethyl sulfoxide; acetone; toluene;
DOI:10.1021/jm020092y