methyl 2,6-anhydro-8-O-benzoyl-3-deoxy-4,5-O-isopropylidene-7-O-<(2-methoxyethoxy)methyl>-D-glycero-D-talo-octanoate

Base Information

Chemical Name:methyl 2,6-anhydro-8-O-benzoyl-3-deoxy-4,5-O-isopropylidene-7-O-<(2-methoxyethoxy)methyl>-D-glycero-D-talo-octanoate
CAS No.:129907-67-1
Molecular Formula:C₂₃H₃₂O₁₀
Molecular Weight:468.501
Hs Code.:

Synonyms:methyl 2,6-anhydro-8-O-benzoyl-3-deoxy-4,5-O-isopropylidene-7-O-<(2-methoxyethoxy)methyl>-D-glycero-D-talo-octanoate

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Chemical Property of methyl 2,6-anhydro-8-O-benzoyl-3-deoxy-4,5-O-isopropylidene-7-O-<(2-methoxyethoxy)methyl>-D-glycero-D-talo-octanoate

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Technology Process of methyl 2,6-anhydro-8-O-benzoyl-3-deoxy-4,5-O-isopropylidene-7-O-<(2-methoxyethoxy)methyl>-D-glycero-D-talo-octanoate

There total 4 articles about methyl 2,6-anhydro-8-O-benzoyl-3-deoxy-4,5-O-isopropylidene-7-O-<(2-methoxyethoxy)methyl>-D-glycero-D-talo-octanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 3970-21-6
2-Methoxyethoxymethyl chloride

: 129916-48-9
methyl 2,6-anhydro-8-O-benzoyl-3-deoxy-4,5-O-isopropylidene-D-glycero-D-talo-octonate

: 129907-67-1
methyl 2,6-anhydro-8-O-benzoyl-3-deoxy-4,5-O-isopropylidene-7-O-<(2-methoxyethoxy)methyl>-D-glycero-D-talo-octanoate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; for 48h; Ambient temperature;
DOI:10.1016/0008-6215(90)84236-N

Reference yield:

: 129907-66-0
methyl 2,6-anhydro-8-O-benzoyl-3-deoxy-D-glycero-D-talo-octonate

: 129907-67-1
methyl 2,6-anhydro-8-O-benzoyl-3-deoxy-4,5-O-isopropylidene-7-O-<(2-methoxyethoxy)methyl>-D-glycero-D-talo-octanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / Dowex 50W * 12(H+) resin / 2 h / Ambient temperature

2: 72 percent / N,N-diisopropylethylamine / CH₂Cl₂ / 48 h / Ambient temperature

With Dowex 50W * 12(H+) resin; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1016/0008-6215(90)84236-N

Reference yield:

: 106174-63-4
methyl 2,6-anhydro-3-deoxy-D-glycero-D-talo-octonate

: 129907-67-1
methyl 2,6-anhydro-8-O-benzoyl-3-deoxy-4,5-O-isopropylidene-7-O-<(2-methoxyethoxy)methyl>-D-glycero-D-talo-octanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 51 percent / pyridine / 1) 1.5 h, 0 deg C, 2) r.t., overnight

2: 100 percent / Dowex 50W * 12(H+) resin / 2 h / Ambient temperature

3: 72 percent / N,N-diisopropylethylamine / CH₂Cl₂ / 48 h / Ambient temperature

With pyridine; Dowex 50W * 12(H+) resin; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1016/0008-6215(90)84236-N