methyl 2,6-anhydro-8-O-benzoyl-3-deoxy-4,5-O-isopropylidene-D-glycero-D-talo-octonate

Base Information

Chemical Name:methyl 2,6-anhydro-8-O-benzoyl-3-deoxy-4,5-O-isopropylidene-D-glycero-D-talo-octonate
CAS No.:129916-48-9
Molecular Formula:C₁₉H₂₄O₈
Molecular Weight:380.395
Hs Code.:

Synonyms:methyl 2,6-anhydro-8-O-benzoyl-3-deoxy-4,5-O-isopropylidene-D-glycero-D-talo-octonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2,6-anhydro-8-O-benzoyl-3-deoxy-4,5-O-isopropylidene-D-glycero-D-talo-octonate

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Technology Process of methyl 2,6-anhydro-8-O-benzoyl-3-deoxy-4,5-O-isopropylidene-D-glycero-D-talo-octonate

There total 3 articles about methyl 2,6-anhydro-8-O-benzoyl-3-deoxy-4,5-O-isopropylidene-D-glycero-D-talo-octonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 129907-66-0
methyl 2,6-anhydro-8-O-benzoyl-3-deoxy-D-glycero-D-talo-octonate

: 67-64-1
acetone

: 129916-48-9
methyl 2,6-anhydro-8-O-benzoyl-3-deoxy-4,5-O-isopropylidene-D-glycero-D-talo-octonate

Guidance literature:: With Dowex 50W * 12(H+) resin; for 2h; Ambient temperature;
DOI:10.1016/0008-6215(90)84236-N

Reference yield:

: 106174-63-4
methyl 2,6-anhydro-3-deoxy-D-glycero-D-talo-octonate

: 129916-48-9
methyl 2,6-anhydro-8-O-benzoyl-3-deoxy-4,5-O-isopropylidene-D-glycero-D-talo-octonate

Guidance literature:: Multi-step reaction with 2 steps

1: 51 percent / pyridine / 1) 1.5 h, 0 deg C, 2) r.t., overnight

2: 100 percent / Dowex 50W * 12(H+) resin / 2 h / Ambient temperature

With pyridine; Dowex 50W * 12(H+) resin;
DOI:10.1016/0008-6215(90)84236-N

Reference yield:

: 98-88-4
benzoyl chloride

: 129916-48-9
methyl 2,6-anhydro-8-O-benzoyl-3-deoxy-4,5-O-isopropylidene-D-glycero-D-talo-octonate

Guidance literature:: Multi-step reaction with 2 steps

1: 51 percent / pyridine / 1) 1.5 h, 0 deg C, 2) r.t., overnight

2: 100 percent / Dowex 50W * 12(H+) resin / 2 h / Ambient temperature

With pyridine; Dowex 50W * 12(H+) resin;
DOI:10.1016/0008-6215(90)84236-N