C₂₄H₂₃F₂NO₃

Base Information

Chemical Name:C₂₄H₂₃F₂NO₃
CAS No.:1427406-59-4
Molecular Formula:C₂₄H₂₃F₂NO₃
Molecular Weight:411.448
Hs Code.:

C<sub>24</sub>H<sub>23</sub>F<sub>2</sub>NO<sub>3</sub>

Synonyms:C₂₄H₂₃F₂NO₃

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Chemical Property of C₂₄H₂₃F₂NO₃

Chemical Property:

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Technology Process of C₂₄H₂₃F₂NO₃

There total 14 articles about C₂₄H₂₃F₂NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1427408-38-5
C₂₇H₂₉F₂NO₃

: 1427406-59-4
C₂₄H₂₃F₂NO₃

Guidance literature:: With water; sodium hydroxide; In tetrahydrofuran; methanol; for 3h;

Reference yield:

: 1227210-35-6
1-bromo-4-fluoro-2-methyl-3-nitro-benzene

: 1427406-59-4
C₂₄H₂₃F₂NO₃

Guidance literature:: Multi-step reaction with 9 steps

1: iron; ammonium chloride / ethanol / 3 h / Reflux

2: dmap; triethylamine / N,N-dimethyl-formamide

3: potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 4 h / 80 °C / Inert atmosphere

4: dihydrogen peroxide; water; sodium hydroxide / tetrahydrofuran / 3 h / 0 - 20 °C

5: trifluoroacetic acid / dichloromethane / 20 °C

6: sodium carbonate / tetrahydrofuran / 3 h / 0 °C

7: borane-THF / tetrahydrofuran / 60 °C / Inert atmosphere

8: caesium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C

9: water; sodium hydroxide / tetrahydrofuran; methanol / 3 h

With dmap; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; borane-THF; water; dihydrogen peroxide; potassium acetate; iron; sodium carbonate; ammonium chloride; caesium carbonate; triethylamine; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: 3013-27-2
1-fluoro-3-methyl-2-nitro-benzene

: 1427406-59-4
C₂₄H₂₃F₂NO₃

Guidance literature:: Multi-step reaction with 10 steps

1: sulfuric acid; N-Bromosuccinimide / 2 h / 20 °C

2: iron; ammonium chloride / ethanol / 3 h / Reflux

3: dmap; triethylamine / N,N-dimethyl-formamide

4: potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 4 h / 80 °C / Inert atmosphere

5: dihydrogen peroxide; water; sodium hydroxide / tetrahydrofuran / 3 h / 0 - 20 °C

6: trifluoroacetic acid / dichloromethane / 20 °C

7: sodium carbonate / tetrahydrofuran / 3 h / 0 °C

8: borane-THF / tetrahydrofuran / 60 °C / Inert atmosphere

9: caesium carbonate / N,N-dimethyl-formamide / 1 h / 20 °C

10: water; sodium hydroxide / tetrahydrofuran; methanol / 3 h

With dmap; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; N-Bromosuccinimide; borane-THF; sulfuric acid; water; dihydrogen peroxide; potassium acetate; iron; sodium carbonate; ammonium chloride; caesium carbonate; triethylamine; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;