m-chlorobenzyl α-disulfone

Base Information

Chemical Name:m-chlorobenzyl α-disulfone
CAS No.:76625-90-6
Molecular Formula:C₁₄H₁₂Cl₂O₄S₂
Molecular Weight:379.285
Hs Code.:

Synonyms:m-chlorobenzyl α-disulfone

Suppliers and Price of m-chlorobenzyl α-disulfone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of m-chlorobenzyl α-disulfone

Chemical Property:

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Technology Process of m-chlorobenzyl α-disulfone

There total 2 articles about m-chlorobenzyl α-disulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: m-chlorobenzyl (m-chlorophenyl)methanethiosulfonate

: 76625-90-6
m-chlorobenzyl α-disulfone

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 120h; Ambient temperature;
DOI:10.1021/ja00395a024

Reference yield:

: 137775-32-7
1,2-bis(3-chlorobenzyl)disulfane

: 76625-90-6
m-chlorobenzyl α-disulfone

Guidance literature:: Multi-step reaction with 2 steps

1: 21 percent / m-chloroperbenzoic acid / CHCl₃ / 21 h / Ambient temperature

2: 27 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 120 h / Ambient temperature

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; chloroform;
DOI:10.1021/ja00395a024

Reference yield:

: 76625-90-6
m-chlorobenzyl α-disulfone

: 459-73-4
GlyOEt*HCl

: (3-Chloro-phenylmethanesulfonylamino)-acetic acid ethyl ester

Guidance literature:: With conjugated acid of glycine ethyl ester; water; In 1,4-dioxane; at 25 ℃; Mechanism; Product distribution; Rate constant;
DOI:10.1021/ja00395a024