Technology Process of C39H46BrF2NO9
There total 5 articles about C39H46BrF2NO9 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethyl borane / tetrahydrofuran; N,N-dimethyl-formamide / 20 °C
2: aluminum isopropoxide / isopropyl alcohol / Reflux; Inert atmosphere
3: dmap; diisopropyl-carbodiimide / Inert atmosphere
With
dmap; triethyl borane; aluminum isopropoxide; diisopropyl-carbodiimide;
In
tetrahydrofuran; N,N-dimethyl-formamide; isopropyl alcohol;
2: Meerwein-Ponndorf-Verley reduction;
DOI:10.1002/chem.201100183
- Guidance literature:
-
Multi-step reaction with 4 steps
1: N-ethyl-N,N-diisopropylamine; tert.-butylhydroperoxide; titanium(IV) isopropylate / dichloromethane; hexane / 3 h / 0 °C / Inert atmosphere
2: boron trifluoride diethyl etherate / N,N-dimethyl-formamide; tetrahydrofuran / 6 h / 20 °C / Inert atmosphere
3: aluminum isopropoxide / isopropyl alcohol / Inert atmosphere; Reflux
4: triethylamine; dmap / tetrahydrofuran / Inert atmosphere
With
titanium(IV) isopropylate; tert.-butylhydroperoxide; dmap; boron trifluoride diethyl etherate; aluminum isopropoxide; triethylamine; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; isopropyl alcohol;
3: |Meerwein-Ponndorf-Verley Reduction;
DOI:10.1002/chem.201302070
