3-<4-(2-methylene-6,6-dimethylcyclohexyl)-3-phenylsulphonylbutyl>-3-methyloxetane

Base Information

Chemical Name:3-<4-(2-methylene-6,6-dimethylcyclohexyl)-3-phenylsulphonylbutyl>-3-methyloxetane
CAS No.:84078-63-7
Molecular Formula:C₂₃H₃₄O₃S
Molecular Weight:390.587
Hs Code.:

Synonyms:3-<4-(2-methylene-6,6-dimethylcyclohexyl)-3-phenylsulphonylbutyl>-3-methyloxetane

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Chemical Property of 3-<4-(2-methylene-6,6-dimethylcyclohexyl)-3-phenylsulphonylbutyl>-3-methyloxetane

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Technology Process of 3-<4-(2-methylene-6,6-dimethylcyclohexyl)-3-phenylsulphonylbutyl>-3-methyloxetane

There total 9 articles about 3-<4-(2-methylene-6,6-dimethylcyclohexyl)-3-phenylsulphonylbutyl>-3-methyloxetane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 84078-62-6
3-(2-iodoethyl)-3-methyloxetane

: 84078-61-5
1-(2-phenylsulphonylethyl)-2-methylene-6,6-dimethylcyclohexane

: 84078-63-7
3-<4-(2-methylene-6,6-dimethylcyclohexyl)-3-phenylsulphonylbutyl>-3-methyloxetane

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; 1.) -78 deg C, 2.) 20 deg C, 2 h;
DOI:10.1039/P19830001783

Reference yield:

: 84078-59-1
2-(2'-Methylene-6',6'-dimethylcyclohexyl)ethanol

: 84078-63-7
3-<4-(2-methylene-6,6-dimethylcyclohexyl)-3-phenylsulphonylbutyl>-3-methyloxetane

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / nBu₃P / CH₂Cl₂ / 0 °C

2: 83 percent / Me₃SiOOSiMe₃ / benzene / 18 h / Heating

3: 78 percent / BuLi / tetrahydrofuran / -78 - 20 °C

With n-butyllithium; tributylphosphine; bis-trimethylsilanyl peroxide; In tetrahydrofuran; dichloromethane; benzene;
DOI:10.1039/c39820001078

Reference yield:

: 84078-60-4
1-(2-phenylthioethyl)-2-methylene-6,6-dimethylcyclohexane

: 84078-63-7
3-<4-(2-methylene-6,6-dimethylcyclohexyl)-3-phenylsulphonylbutyl>-3-methyloxetane

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / Me₃SiOOSiMe₃ / benzene / 18 h / Heating

2: 78 percent / BuLi / tetrahydrofuran / -78 - 20 °C

With n-butyllithium; bis-trimethylsilanyl peroxide; In tetrahydrofuran; benzene;
DOI:10.1039/c39820001078