Technology Process of C21H26N2O2
There total 5 articles about C21H26N2O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
oxygen; palladium diacetate; sodium triflate; potassium carbonate;
In
3-methylpentan-3-ol;
at 135 ℃;
for 36h;
under 760.051 Torr;
regioselective reaction;
DOI:10.1021/ol201930e
- Guidance literature:
-
Multi-step reaction with 4 steps
1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C
2: boron tribromide / dichloromethane / 24 h / 20 °C
3: potassium carbonate / N,N-dimethyl-formamide / 24 h / 20 °C
4: oxygen; palladium diacetate; sodium triflate; potassium carbonate / 3-methylpentan-3-ol / 36 h / 135 °C / 760.05 Torr
With
oxygen; palladium diacetate; sodium triflate; boron tribromide; potassium carbonate; N-ethyl-N,N-diisopropylamine;
In
dichloromethane; 3-methylpentan-3-ol; N,N-dimethyl-formamide;
DOI:10.1021/ol201930e
- Guidance literature:
-
Multi-step reaction with 3 steps
1: boron tribromide / dichloromethane / 24 h / 20 °C
2: potassium carbonate / N,N-dimethyl-formamide / 24 h / 20 °C
3: oxygen; palladium diacetate; sodium triflate; potassium carbonate / 3-methylpentan-3-ol / 36 h / 135 °C / 760.05 Torr
With
oxygen; palladium diacetate; sodium triflate; boron tribromide; potassium carbonate;
In
dichloromethane; 3-methylpentan-3-ol; N,N-dimethyl-formamide;
DOI:10.1021/ol201930e
