3,2',4',6'-tetrakis(benzyloxy)-4-methoxychalcone

Base Information

Chemical Name:3,2',4',6'-tetrakis(benzyloxy)-4-methoxychalcone
CAS No.:114057-73-7
Molecular Formula:C₄₄H₃₈O₆
Molecular Weight:662.782
Hs Code.:

Synonyms:3,2',4',6'-tetrakis(benzyloxy)-4-methoxychalcone

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Chemical Property of 3,2',4',6'-tetrakis(benzyloxy)-4-methoxychalcone

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of 3,2',4',6'-tetrakis(benzyloxy)-4-methoxychalcone

There total 1 articles about 3,2',4',6'-tetrakis(benzyloxy)-4-methoxychalcone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 520-33-2,41001-90-5,69097-99-0
(S)-2,3-dihydro-5,7-dihydroxy-2-(3-hydroxy-4-methoxyphenyl)-4-benzopyrone

: 100-44-7
benzyl chloride

: 114057-73-7
3,2',4',6'-tetrakis(benzyloxy)-4-methoxychalcone

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 120 ℃; for 5h;
DOI:10.1021/jm00401a030

Reference yield: 89.3%

: 114057-73-7
3,2',4',6'-tetrakis(benzyloxy)-4-methoxychalcone

: 76260-66-7
α,β-epoxy-3,2',4',6'-tetrakis(benzyloxy)-4-methoxychalcone

Guidance literature:: With sodium hydroxide; dihydrogen peroxide; In methanol; chloroform; for 18h; Ambient temperature;
DOI:10.1021/jm00401a030

Reference yield:

: 114057-73-7
3,2',4',6'-tetrakis(benzyloxy)-4-methoxychalcone

: 70411-27-7,82517-11-1,114179-12-3
3,5,7,3'-tetrahydroxy-4'-methoxyflavanone

Guidance literature:: Multi-step reaction with 2 steps

1: 89.3 percent / 7.1 N NaOH, 30percent H₂O₂ / CHCl₃; methanol / 18 h / Ambient temperature

2: 88 percent / HCl, H₂ / Pd/C / dimethylformamide / 4 h

With hydrogenchloride; sodium hydroxide; hydrogen; dihydrogen peroxide; palladium on activated charcoal; In methanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1021/jm00401a030