C₃₀H₃₂N₈O₄

Base Information

Chemical Name:C₃₀H₃₂N₈O₄
CAS No.:1612874-01-7
Molecular Formula:C₃₀H₃₂N₈O₄
Molecular Weight:568.635
Hs Code.:

C<sub>30</sub>H<sub>32</sub>N<sub>8</sub>O<sub>4</sub>

Synonyms:C₃₀H₃₂N₈O₄

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Chemical Property of C₃₀H₃₂N₈O₄

Chemical Property:

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Technology Process of C₃₀H₃₂N₈O₄

There total 8 articles about C₃₀H₃₂N₈O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 1612874-00-6
C₂₇H₃₂N₈O₃

: 471-25-0
Propiolic acid

: 1612874-01-7
C₃₀H₃₂N₈O₄

Guidance literature:: Propiolic acid; With dicyclohexyl-carbodiimide; In dichloromethane; for 0.166667h;

C₂₇H₃₂N₈O₃; With dmap; In dichloromethane; for 0.5h;
DOI:10.1002/ejoc.201301838

Reference yield:

: 6310-19-6
4-tert-butyl-2-nitroaniline

: 1612874-01-7
C₃₀H₃₂N₈O₄

Guidance literature:: Multi-step reaction with 6 steps

1.1: Iodine monochloride / 1,2-dichloro-ethane / 3 h / 70 °C / Inert atmosphere

2.1: sodium nitrite; sulfuric acid / ethanol / 0 °C / Reflux

3.1: tin(II) chloride dihdyrate; ethanol / Reflux

4.1: sodium azide; sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; copper(l) iodide; N,N`-dimethylethylenediamine / dimethyl sulfoxide; water / 1 h / 20 °C

5.1: sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; copper(II) sulfate / water; tetrahydrofuran / 12 h / 20 °C

6.1: dicyclohexyl-carbodiimide / dichloromethane / 0.17 h

6.2: 0.5 h

With copper(l) iodide; sodium azide; sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; tin(II) chloride dihdyrate; ethanol; sulfuric acid; Iodine monochloride; copper(II) sulfate; dicyclohexyl-carbodiimide; N,N`-dimethylethylenediamine; sodium nitrite; In tetrahydrofuran; ethanol; dichloromethane; water; dimethyl sulfoxide; 1,2-dichloro-ethane;
DOI:10.1002/ejoc.201301838

Reference yield:

: 1369827-82-6
C₁₀H₁₂INO₂

: 1612874-01-7
C₃₀H₃₂N₈O₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: tin(II) chloride dihdyrate; ethanol / Reflux

2.1: sodium azide; sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; copper(l) iodide; N,N`-dimethylethylenediamine / dimethyl sulfoxide; water / 1 h / 20 °C

3.1: sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; copper(II) sulfate / water; tetrahydrofuran / 12 h / 20 °C

4.1: dicyclohexyl-carbodiimide / dichloromethane / 0.17 h

4.2: 0.5 h

With copper(l) iodide; sodium azide; sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; tin(II) chloride dihdyrate; ethanol; copper(II) sulfate; dicyclohexyl-carbodiimide; N,N`-dimethylethylenediamine; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide;
DOI:10.1002/ejoc.201301838