methyl 5-acetamido-2,6-anhydro-4-O-benzoyl-7-O-(tert-butyldimethylsilyl)-3,5-dideoxy-8,9-O-isopropylidene-D-glycero-D-galacto-non-2-enoate

Base Information

Chemical Name:methyl 5-acetamido-2,6-anhydro-4-O-benzoyl-7-O-(tert-butyldimethylsilyl)-3,5-dideoxy-8,9-O-isopropylidene-D-glycero-D-galacto-non-2-enoate
CAS No.:1171908-44-3
Molecular Formula:C₂₈H₄₁NO₉Si
Molecular Weight:563.72
Hs Code.:

Synonyms:methyl 5-acetamido-2,6-anhydro-4-O-benzoyl-7-O-(tert-butyldimethylsilyl)-3,5-dideoxy-8,9-O-isopropylidene-D-glycero-D-galacto-non-2-enoate

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Chemical Property of methyl 5-acetamido-2,6-anhydro-4-O-benzoyl-7-O-(tert-butyldimethylsilyl)-3,5-dideoxy-8,9-O-isopropylidene-D-glycero-D-galacto-non-2-enoate

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Technology Process of methyl 5-acetamido-2,6-anhydro-4-O-benzoyl-7-O-(tert-butyldimethylsilyl)-3,5-dideoxy-8,9-O-isopropylidene-D-glycero-D-galacto-non-2-enoate

There total 1 articles about methyl 5-acetamido-2,6-anhydro-4-O-benzoyl-7-O-(tert-butyldimethylsilyl)-3,5-dideoxy-8,9-O-isopropylidene-D-glycero-D-galacto-non-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 69739-34-0
t-butyldimethylsiyl triflate

: 134699-92-6
methyl 5-acetamido-2,6-anhydro-4-O-benzoyl-3,5-dideoxy-8,9-O-isopropylidene-D-glycero-D-galacto-non-2-enoate

: 1171908-44-3
methyl 5-acetamido-2,6-anhydro-4-O-benzoyl-7-O-(tert-butyldimethylsilyl)-3,5-dideoxy-8,9-O-isopropylidene-D-glycero-D-galacto-non-2-enoate

Guidance literature:: With lutidine; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1002/chem.200900093

Reference yield: 97.0%

: 1171908-44-3
methyl 5-acetamido-2,6-anhydro-4-O-benzoyl-7-O-(tert-butyldimethylsilyl)-3,5-dideoxy-8,9-O-isopropylidene-D-glycero-D-galacto-non-2-enoate

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 1616503-10-6
1-C-[methyl(5-acetamido-2,6-anhydro-7-O-tert-butyldimethylsilyloxy-3,5-dideoxy-8,9-O-isopropylidene-D-glycero-α-D-galacto-nonulosyl)-3-enoate]cyclohexanol

Guidance literature:: With samarium diiodide; In tetrahydrofuran; at -78 - 20 ℃; for 1h; regioselective reaction; Inert atmosphere;
DOI:10.1002/anie.201402891

Reference yield: 89.0%

: 1171908-44-3
methyl 5-acetamido-2,6-anhydro-4-O-benzoyl-7-O-(tert-butyldimethylsilyl)-3,5-dideoxy-8,9-O-isopropylidene-D-glycero-D-galacto-non-2-enoate

: 100-46-9
benzylamine

: 1171908-74-9
methyl 5-acetamido-2,6-anhydro-4-(benzylamino)-7-O-(tert-butyldimethylsilyl)-3,4,5-trideoxy-8,9-O-isopropylidene-D-glycero-D-galacto-non-2-enoate

Guidance literature:: With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; triethylamine; 1,4-di(diphenylphosphino)-butane; In dichloromethane; at 60 - 80 ℃; regioselective reaction; Inert atmosphere;
DOI:10.1002/chem.200900093