methyl 5-acetamido-2,6-anhydro-7-O-(tert-butyldimethylsilyl)-3,4,5-trideoxy-8,9-O-isopropylidene-4-C-[bis(phenylsulfonyl)methyl]-D-glycero-D-galacto-non-2-enoate

Base Information

Chemical Name:methyl 5-acetamido-2,6-anhydro-7-O-(tert-butyldimethylsilyl)-3,4,5-trideoxy-8,9-O-isopropylidene-4-C-[bis(phenylsulfonyl)methyl]-D-glycero-D-galacto-non-2-enoate
CAS No.:1171908-65-8
Molecular Formula:C₃₄H₄₇NO₁₁S₂Si
Molecular Weight:737.965
Hs Code.:

methyl 5-acetamido-2,6-anhydro-7-O-(tert-butyldimethylsilyl)-3,4,5-trideoxy-8,9-O-isopropylidene-4-C-[bis(phenylsulfonyl)methyl]-D-glycero-D-galacto-non-2-enoate

Synonyms:methyl 5-acetamido-2,6-anhydro-7-O-(tert-butyldimethylsilyl)-3,4,5-trideoxy-8,9-O-isopropylidene-4-C-[bis(phenylsulfonyl)methyl]-D-glycero-D-galacto-non-2-enoate

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Chemical Property of methyl 5-acetamido-2,6-anhydro-7-O-(tert-butyldimethylsilyl)-3,4,5-trideoxy-8,9-O-isopropylidene-4-C-[bis(phenylsulfonyl)methyl]-D-glycero-D-galacto-non-2-enoate

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Technology Process of methyl 5-acetamido-2,6-anhydro-7-O-(tert-butyldimethylsilyl)-3,4,5-trideoxy-8,9-O-isopropylidene-4-C-[bis(phenylsulfonyl)methyl]-D-glycero-D-galacto-non-2-enoate

There total 2 articles about methyl 5-acetamido-2,6-anhydro-7-O-(tert-butyldimethylsilyl)-3,4,5-trideoxy-8,9-O-isopropylidene-4-C-[bis(phenylsulfonyl)methyl]-D-glycero-D-galacto-non-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 1171908-44-3
methyl 5-acetamido-2,6-anhydro-4-O-benzoyl-7-O-(tert-butyldimethylsilyl)-3,5-dideoxy-8,9-O-isopropylidene-D-glycero-D-galacto-non-2-enoate

: 3406-02-8
bis(phenylsulfonyl)methane

: 1171908-65-8
methyl 5-acetamido-2,6-anhydro-7-O-(tert-butyldimethylsilyl)-3,4,5-trideoxy-8,9-O-isopropylidene-4-C-[bis(phenylsulfonyl)methyl]-D-glycero-D-galacto-non-2-enoate

Guidance literature:: With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; tributylphosphine; sodium; In tetrahydrofuran; mineral oil; at 80 ℃; for 15h; stereoselective reaction; Inert atmosphere;
DOI:10.1002/ejoc.200901452

Reference yield: 46.0%

: 1171908-44-3
methyl 5-acetamido-2,6-anhydro-4-O-benzoyl-7-O-(tert-butyldimethylsilyl)-3,5-dideoxy-8,9-O-isopropylidene-D-glycero-D-galacto-non-2-enoate

: NaCH(SO₂Ph)2

: 1171908-65-8
methyl 5-acetamido-2,6-anhydro-7-O-(tert-butyldimethylsilyl)-3,4,5-trideoxy-8,9-O-isopropylidene-4-C-[bis(phenylsulfonyl)methyl]-D-glycero-D-galacto-non-2-enoate

Guidance literature:: With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; tributylphosphine; In tetrahydrofuran; at 60 - 80 ℃; regioselective reaction; Inert atmosphere;
DOI:10.1002/chem.200900093