Spiro[5.6]dodecan-7-ol

Base Information

• Chemical Name: Spiro[5.6]dodecan-7-ol
• CAS No.: 1130-20-7
• Molecular Formula: C₁₂H₂₂O
• Molecular Weight: 182.306
• Hs Code.: 2906199090
• European Community (EC) Number: 601-221-0
• DSSTox Substance ID: DTXSID90862558
• Nikkaji Number: J1.552.258E
• Mol file: 1130-20-7.mol

Synonyms:spiro[5.6]dodecan-7-ol;1130-20-7;Spiro5.6dodecan-7-ol;spiro[5.6]dodecan-12-ol;Spiro(5.6)dodecan-7-ol;Spiro[5.6]dodecane-7-ol;DTXSID90862558;FT-0730623

Chemical Property of Spiro[5.6]dodecan-7-ol

Chemical Property:

• Vapor Pressure: 0.00237mmHg at 25°C
• Boiling Point: 256.1°Cat760mmHg
• Flash Point: 105.9°C
• PSA: 20.23000
• Density: 0.97g/cm³
• LogP: 3.26190
• XLogP3: 3.8
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 182.167065321
• Heavy Atom Count: 13
• Complexity: 159

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CCC(C2(CC1)CCCCC2)O

Technology Process of Spiro[5.6]dodecan-7-ol

There total 5 articles about Spiro[5.6]dodecan-7-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C12H20O → spiro[5.6]dodecan-8-ol + Spiro<5.6>dodecan-7-ol (1130-20-7)

Guidance literature:

With manganese; crithmene; 2,4,6-collidine hydrochloride; bis(cyclopentadienyl)titanium dichloride; In tetrahydrofuran; at 20 ℃; for 16h; Further Variations:; Reagents; Product distribution;

DOI:10.1021/ja067054e

Reference yield:

→ Spiro<5.6>dodecan-7-ol (1130-20-7)

Guidance literature:

With nickel; at 100 ℃; under 73550.8 Torr; Hydrogenation;

Reference yield:

spiro[5.6]dodecan-7-one (4728-90-9) → Spiro<5.6>dodecan-7-ol (1130-20-7)

Guidance literature:

With lithium aluminium tetrahydride; diethyl ether;

upstream raw materials:

spiro[5.6]dodecan-7-one

1,5-dibromo-pentane

cycloheptanone

Downstream raw materials:

1-cyclohexyl-1-cyclohexene

[1,1';1',1'';1'',1''']quatercyclohexane