2,4,6-Cycloheptatrien-1-yl(4-methoxyphenyl)(trimethylsiloxy)acetonitril

Base Information

Chemical Name:2,4,6-Cycloheptatrien-1-yl(4-methoxyphenyl)(trimethylsiloxy)acetonitril
CAS No.:97847-92-2
Molecular Formula:C₁₉H₂₃NO₂Si
Molecular Weight:325.483
Hs Code.:

Synonyms:2,4,6-Cycloheptatrien-1-yl(4-methoxyphenyl)(trimethylsiloxy)acetonitril

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Chemical Property of 2,4,6-Cycloheptatrien-1-yl(4-methoxyphenyl)(trimethylsiloxy)acetonitril

Chemical Property:

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Technology Process of 2,4,6-Cycloheptatrien-1-yl(4-methoxyphenyl)(trimethylsiloxy)acetonitril

There total 1 articles about 2,4,6-Cycloheptatrien-1-yl(4-methoxyphenyl)(trimethylsiloxy)acetonitril which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 66985-48-6
2-(4-methoxyphenyl)-2-(trimethylsilyloxy)acetonitrile

: 27081-10-3
tropylium tetrafluoroborate

: 97847-92-2
2,4,6-Cycloheptatrien-1-yl(4-methoxyphenyl)(trimethylsiloxy)acetonitril

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; - 78 deg C to r.t.;

Reference yield: 82.0%

: 97847-92-2
2,4,6-Cycloheptatrien-1-yl(4-methoxyphenyl)(trimethylsiloxy)acetonitril

: 97847-94-4
2,4,6-Cycloheptatrien-1-yl-(4-methoxyphenyl)keton

Guidance literature:: With triethylamine hydrofluoride;
DOI:10.1016/S0040-4039(00)94871-8

Reference yield:

: 97847-92-2
2,4,6-Cycloheptatrien-1-yl(4-methoxyphenyl)(trimethylsiloxy)acetonitril

: 104876-73-5
anti-3-(4-Methoxybenzoyl)-N-methyl-6,7-diaza-exo-tricyclo<3.2.2.0^2,4>non-8-en-6,7-dicarboximid

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / NEt₃HF / tetrahydrofuran / Ambient temperature

2: 88 percent / CH₂Cl₂ / 1) 0 deg C, 10 min, 2) r.t., 30 min

With triethylamine hydrofluoride; In tetrahydrofuran; dichloromethane;