PhCH₂OSiH₂Ph

Base Information

• Chemical Name: PhCH₂OSiH₂Ph
• CAS No.: 1015477-65-2
• Molecular Formula: C₁₃H₁₄OSi
• Molecular Weight: 214.339
• Mol file: 1015477-65-2.mol

Synonyms:PhCH₂OSiH₂Ph

Chemical Property of PhCH₂OSiH₂Ph

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of PhCH₂OSiH₂Ph

There total 11 articles about PhCH₂OSiH₂Ph which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

phenylsilane (694-53-1) + benzyl alcohol (100-51-6,185532-71-2) → PhCH2OSiH2Ph (1015477-65-2)

Guidance literature:

With iron(II)β-diketiminate complex; In benzene-d6; at 20 ℃; for 18h;

DOI:10.1021/acscatal.0c01440

Reference yield: 95.0%

phenylsilane (694-53-1) + benzaldehyde (100-52-7) → PhCH2OSiH2Ph (1015477-65-2) + di(benzyloxy)phenylsilane (18641-08-2) + tri(benzyloxy)phenylsilane + benzyl alcohol (100-51-6,185532-71-2)

Guidance literature:

With MnN(salen-3,5-tBu₂); In [D₃]acetonitrile; at 80 ℃; for 3.3h; Solvent; Temperature; Time; Concentration; Mechanism; Sealed tube;

DOI:10.1021/om400805v

Reference yield: 95.0%

phenylsilane (694-53-1) + benzaldehyde (100-52-7) → PhCH2OSiH2Ph (1015477-65-2)

Guidance literature:

With Ni(η⁵-C₅H₅)Cl(Mes-NHC)-CH₂-C₆H₄-Si(OMe)₃; In tetrahydrofuran; at 25 ℃; for 22h; Reagent/catalyst; Schlenk technique;

DOI:10.1039/c9cc05379d

upstream raw materials:

phenylsilane

benzaldehyde

Phenyltrichlorosilane

phenylsilane-d3

Downstream raw materials:

benzyl alcohol