(5S,8S)-2,4-dioxo-1,3,7-triazaspiro[4.5]decane-1,3,7,8-tetracarboxylic acid 7-benzyl ester 1,3,8-tert-butyl ester

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Chemical Name:(5S,8S)-2,4-dioxo-1,3,7-triazaspiro[4.5]decane-1,3,7,8-tetracarboxylic acid 7-benzyl ester 1,3,8-tert-butyl ester
CAS No.:862177-21-7
Molecular Formula:C₃₀H₄₁N₃O₁₀
Molecular Weight:603.67
Hs Code.:

Synonyms:(5S,8S)-2,4-dioxo-1,3,7-triazaspiro[4.5]decane-1,3,7,8-tetracarboxylic acid 7-benzyl ester 1,3,8-tert-butyl ester

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Chemical Property of (5S,8S)-2,4-dioxo-1,3,7-triazaspiro[4.5]decane-1,3,7,8-tetracarboxylic acid 7-benzyl ester 1,3,8-tert-butyl ester

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Technology Process of (5S,8S)-2,4-dioxo-1,3,7-triazaspiro[4.5]decane-1,3,7,8-tetracarboxylic acid 7-benzyl ester 1,3,8-tert-butyl ester

There total 2 articles about (5S,8S)-2,4-dioxo-1,3,7-triazaspiro[4.5]decane-1,3,7,8-tetracarboxylic acid 7-benzyl ester 1,3,8-tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 147489-30-3
(2S)-5-oxopiperidine-1,2-dicarboxylic acid 1-benzyl ester 2-tert-butyl ester

: 862177-21-7
(5S,8S)-2,4-dioxo-1,3,7-triazaspiro[4.5]decane-1,3,7,8-tetracarboxylic acid 7-benzyl ester 1,3,8-tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: KCN / dimethylformamide; H₂O / 4 h / 60 °C

2: 2.6 g / DMAP / tetrahydrofuran / 3 h / 20 °C

With dmap; potassium cyanide; In tetrahydrofuran; water; N,N-dimethyl-formamide; 1: Bucherer-Bergs reaction;
DOI:10.1021/ol0507672