ethylthio 2-O-benzoyl-4,6-O-benzylidene-3-O-(4,6-O-benzylidene-2,3-di-O-levulinoyl-β-D-glucopyranosyl)-β-D-glucopyranoside

Base Information

Chemical Name:ethylthio 2-O-benzoyl-4,6-O-benzylidene-3-O-(4,6-O-benzylidene-2,3-di-O-levulinoyl-β-D-glucopyranosyl)-β-D-glucopyranoside
CAS No.:1259035-92-1
Molecular Formula:C₄₅H₅₀O₁₅S
Molecular Weight:862.949
Hs Code.:

Synonyms:ethylthio 2-O-benzoyl-4,6-O-benzylidene-3-O-(4,6-O-benzylidene-2,3-di-O-levulinoyl-β-D-glucopyranosyl)-β-D-glucopyranoside

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Chemical Property of ethylthio 2-O-benzoyl-4,6-O-benzylidene-3-O-(4,6-O-benzylidene-2,3-di-O-levulinoyl-β-D-glucopyranosyl)-β-D-glucopyranoside

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Technology Process of ethylthio 2-O-benzoyl-4,6-O-benzylidene-3-O-(4,6-O-benzylidene-2,3-di-O-levulinoyl-β-D-glucopyranosyl)-β-D-glucopyranoside

There total 1 articles about ethylthio 2-O-benzoyl-4,6-O-benzylidene-3-O-(4,6-O-benzylidene-2,3-di-O-levulinoyl-β-D-glucopyranosyl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1259035-91-0
ethylthio 4,6-O-benzylidene-3-O-(4,6-O-benzylidene-2,3-di-O-levulinyl-β-D-glucopyranosyl)-β-D-glucopyranoside

: 98-88-4
benzoyl chloride

: 1259035-92-1
ethylthio 2-O-benzoyl-4,6-O-benzylidene-3-O-(4,6-O-benzylidene-2,3-di-O-levulinoyl-β-D-glucopyranosyl)-β-D-glucopyranoside

Guidance literature:: With pyridine; dmap; at 120 ℃; for 4h;
DOI:10.1016/j.bmc.2012.04.017

Reference yield: 99.0%

: 1259035-92-1
ethylthio 2-O-benzoyl-4,6-O-benzylidene-3-O-(4,6-O-benzylidene-2,3-di-O-levulinoyl-β-D-glucopyranosyl)-β-D-glucopyranoside

: 1259035-94-3
ethyl 4,6-O-benzylidene-β-D-glucopyranosyl-(1→3)-2-O-benzoyl-4,6-O-benzylidene-1-thio-β-D-glucopyranoside

Guidance literature:: With hydrazine hydrate; acetic acid; In tetrahydrofuran; at 0 ℃; for 0.333333h;
DOI:10.1016/j.bmc.2012.04.017

Reference yield: 82.0%

: 1259035-92-1
ethylthio 2-O-benzoyl-4,6-O-benzylidene-3-O-(4,6-O-benzylidene-2,3-di-O-levulinoyl-β-D-glucopyranosyl)-β-D-glucopyranoside

: 1385068-41-6
2-O-benzoyl-4,6-O-benzylidene-3-O-(4,6-O-benzylidene-2,3-di-O-levulinoyl-β-D-glucopyranosyl)-β-D-glucopyranosyl azide

Guidance literature:: ethylthio 2-O-benzoyl-4,6-O-benzylidene-3-O-(4,6-O-benzylidene-2,3-di-O-levulinoyl-β-D-glucopyranosyl)-β-D-glucopyranoside; With iodine(I) bromide; In dichloromethane; at -78 - 0 ℃; for 0.5h; Molecular sieve; Inert atmosphere;

With sodium azide; In N,N-dimethyl-formamide; at 20 ℃; for 3h;
DOI:10.1016/j.tetlet.2012.05.111