10-(3,4-dihydroxy-phenyl)-9H-furo[3',4':6,7]naphtho[1,2-d][1,3]dioxol-7-one

Base Information

Chemical Name:10-(3,4-dihydroxy-phenyl)-9H-furo[3',4':6,7]naphtho[1,2-d][1,3]dioxol-7-one
CAS No.:203936-81-6
Molecular Formula:C₁₉H₁₂O₆
Molecular Weight:336.301
Hs Code.:

Synonyms:10-(3,4-dihydroxy-phenyl)-9H-furo[3',4':6,7]naphtho[1,2-d][1,3]dioxol-7-one

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Chemical Property of 10-(3,4-dihydroxy-phenyl)-9H-furo[3',4':6,7]naphtho[1,2-d][1,3]dioxol-7-one

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Technology Process of 10-(3,4-dihydroxy-phenyl)-9H-furo[3',4':6,7]naphtho[1,2-d][1,3]dioxol-7-one

There total 1 articles about 10-(3,4-dihydroxy-phenyl)-9H-furo[3',4':6,7]naphtho[1,2-d][1,3]dioxol-7-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1219694-08-2
10-(3,4-bis-benzyloxy-phenyl)-9H-furo[3',4':6,7]naphtho[1,2-d][1,3]dioxol-7-one

: 203936-81-6
10-(3,4-dihydroxy-phenyl)-9H-furo[3',4':6,7]naphtho[1,2-d][1,3]dioxol-7-one

Guidance literature:: 10-(3,4-bis-benzyloxy-phenyl)-9H-furo[3',4':6,7]naphtho[1,2-d][1,3]dioxol-7-one; With boron tribromide; In dichloromethane; at -78 ℃; under 760.051 Torr; Inert atmosphere;

With methanol; In dichloromethane; at -78 - 20 ℃; under 760.051 Torr; Inert atmosphere;
DOI:10.1016/j.bmc.2009.12.038

Reference yield: 89.0%

: 203936-81-6
10-(3,4-dihydroxy-phenyl)-9H-furo[3',4':6,7]naphtho[1,2-d][1,3]dioxol-7-one

: 1428438-85-0
C₁₉H₁₆O₆

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.bmc.2012.11.037

Reference yield:

: 203936-81-6
10-(3,4-dihydroxy-phenyl)-9H-furo[3',4':6,7]naphtho[1,2-d][1,3]dioxol-7-one

: 1428438-87-2
C₂₅H₂₂O₉

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

2: pyridine / 12 h / 20 °C / Inert atmosphere

With pyridine; lithium aluminium tetrahydride; In tetrahydrofuran;
DOI:10.1016/j.bmc.2012.11.037