10-(3,4-bis-benzyloxy-phenyl)-9H-furo[3',4':6,7]naphtho[1,2-d][1,3]dioxol-7-one

Base Information

Chemical Name:10-(3,4-bis-benzyloxy-phenyl)-9H-furo[3',4':6,7]naphtho[1,2-d][1,3]dioxol-7-one
CAS No.:1219694-08-2
Molecular Formula:C₃₃H₂₄O₆
Molecular Weight:516.55
Hs Code.:

Synonyms:10-(3,4-bis-benzyloxy-phenyl)-9H-furo[3',4':6,7]naphtho[1,2-d][1,3]dioxol-7-one

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Chemical Property of 10-(3,4-bis-benzyloxy-phenyl)-9H-furo[3',4':6,7]naphtho[1,2-d][1,3]dioxol-7-one

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Technology Process of 10-(3,4-bis-benzyloxy-phenyl)-9H-furo[3',4':6,7]naphtho[1,2-d][1,3]dioxol-7-one

There total 1 articles about 10-(3,4-bis-benzyloxy-phenyl)-9H-furo[3',4':6,7]naphtho[1,2-d][1,3]dioxol-7-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1219693-99-8
10-(3,4-bis-benzyloxy-phenyl)-furo[3',4':6,7]naphtho[1,2-d][1,3]dioxole-7,9-dione

: 1219694-09-3
10-(3,4-bis-benzyloxyphenyl)-7H-furo[3',4':6,7]naphtho[1,2-d][1,3]dioxol-9-one

: 1219694-08-2
10-(3,4-bis-benzyloxy-phenyl)-9H-furo[3',4':6,7]naphtho[1,2-d][1,3]dioxol-7-one

Guidance literature:: 10-(3,4-bis-benzyloxy-phenyl)-furo[3',4':6,7]naphtho[1,2-d][1,3]dioxole-7,9-dione; With sodium tetrahydroborate; In tetrahydrofuran; at 20 ℃; under 760.051 Torr; Inert atmosphere;

With hydrogenchloride; water; In tetrahydrofuran; under 760.051 Torr; Inert atmosphere;
DOI:10.1016/j.bmc.2009.12.038

Reference yield: 77.0%

: 1219694-08-2
10-(3,4-bis-benzyloxy-phenyl)-9H-furo[3',4':6,7]naphtho[1,2-d][1,3]dioxol-7-one

: 203936-81-6
10-(3,4-dihydroxy-phenyl)-9H-furo[3',4':6,7]naphtho[1,2-d][1,3]dioxol-7-one

Guidance literature:: 10-(3,4-bis-benzyloxy-phenyl)-9H-furo[3',4':6,7]naphtho[1,2-d][1,3]dioxol-7-one; With boron tribromide; In dichloromethane; at -78 ℃; under 760.051 Torr; Inert atmosphere;

With methanol; In dichloromethane; at -78 - 20 ℃; under 760.051 Torr; Inert atmosphere;
DOI:10.1016/j.bmc.2009.12.038

Reference yield:

: 1219694-08-2
10-(3,4-bis-benzyloxy-phenyl)-9H-furo[3',4':6,7]naphtho[1,2-d][1,3]dioxol-7-one

: 1428438-85-0
C₁₉H₁₆O₆

Guidance literature:: Multi-step reaction with 2 steps

1: boron tribromide / dichloromethane / 2 h / -78 °C / Inert atmosphere

2: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

With lithium aluminium tetrahydride; boron tribromide; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmc.2012.11.037