3,2'-Di-N-(benzyloxycarbonyl)-3'-O-(tetrahydropyranyl)-2'',3'',5''-tri-O-acetyl-1,6:6',4'-N,O-carbonylthioribostamycin

Base Information

Chemical Name:3,2'-Di-N-(benzyloxycarbonyl)-3'-O-(tetrahydropyranyl)-2'',3'',5''-tri-O-acetyl-1,6:6',4'-N,O-carbonylthioribostamycin
CAS No.:78763-86-7
Molecular Formula:C₄₆H₅₆N₄O₁₉S
Molecular Weight:1001.03
Hs Code.:

Synonyms:3,2'-Di-N-(benzyloxycarbonyl)-3'-O-(tetrahydropyranyl)-2'',3'',5''-tri-O-acetyl-1,6:6',4'-N,O-carbonylthioribostamycin

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Chemical Property of 3,2'-Di-N-(benzyloxycarbonyl)-3'-O-(tetrahydropyranyl)-2'',3'',5''-tri-O-acetyl-1,6:6',4'-N,O-carbonylthioribostamycin

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Technology Process of 3,2'-Di-N-(benzyloxycarbonyl)-3'-O-(tetrahydropyranyl)-2'',3'',5''-tri-O-acetyl-1,6:6',4'-N,O-carbonylthioribostamycin

There total 1 articles about 3,2'-Di-N-(benzyloxycarbonyl)-3'-O-(tetrahydropyranyl)-2'',3'',5''-tri-O-acetyl-1,6:6',4'-N,O-carbonylthioribostamycin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 66787-83-5
O⁴-(6-amino-2-benzyloxycarbonylamino-N⁶,O⁴-carbonyl-O³-(Ξ)-tetrahydropyran-2-yl-α-D-2,6-dideoxy-glucopyranosyl)-N³-benzyloxycarbonyl-N¹,O⁶-carbonyl-1D-2-deoxy-streptamine

: 59042-15-8
2,3,5-tri-O-acetyl-D-4-thioribofuranosyl chloride

: 78763-86-7
3,2'-Di-N-(benzyloxycarbonyl)-3'-O-(tetrahydropyranyl)-2'',3'',5''-tri-O-acetyl-1,6:6',4'-N,O-carbonylthioribostamycin

Guidance literature:: With calcium sulfate; mercury(II) cyanide; In dichloromethane; for 96h; Heating;
DOI:10.1021/jo00334a042

Reference yield:

: 78763-86-7
3,2'-Di-N-(benzyloxycarbonyl)-3'-O-(tetrahydropyranyl)-2'',3'',5''-tri-O-acetyl-1,6:6',4'-N,O-carbonylthioribostamycin

: 78763-88-9
4''-Thioribostamycin

Guidance literature:: With barium dihydroxide; palladium on activated charcoal; hydrogen; acetic acid; Yield given. Multistep reaction; 1.) dioxane, 60 deg C, 6 h, 2.) dioxane, water;
DOI:10.1021/jo00334a042