4''-Thioribostamycin

Base Information

Chemical Name:4''-Thioribostamycin
CAS No.:78763-88-9
Molecular Formula:2CH₂O₃*C₁₇H₃₄N₄O₉S
Molecular Weight:594.595
Hs Code.:

Synonyms:

Suppliers and Price of 4''-Thioribostamycin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4''-Thioribostamycin

Chemical Property:

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Technology Process of 4''-Thioribostamycin

There total 3 articles about 4''-Thioribostamycin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 66787-83-5
O⁴-(6-amino-2-benzyloxycarbonylamino-N⁶,O⁴-carbonyl-O³-(Ξ)-tetrahydropyran-2-yl-α-D-2,6-dideoxy-glucopyranosyl)-N³-benzyloxycarbonyl-N¹,O⁶-carbonyl-1D-2-deoxy-streptamine

: 78763-88-9
4''-Thioribostamycin

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent / mercuric cyanide, Drierite / CH₂Cl₂ / 96 h / Heating

2: 1.) 1M aq. BaOH, 2.) H₂, Pd/C, AcOH / 1.) dioxane, 60 deg C, 6 h, 2.) dioxane, water

With calcium sulfate; barium dihydroxide; palladium on activated charcoal; hydrogen; mercury(II) cyanide; acetic acid; In dichloromethane;
DOI:10.1021/jo00334a042

Reference yield:

: 59042-15-8
2,3,5-tri-O-acetyl-D-4-thioribofuranosyl chloride

: 78763-88-9
4''-Thioribostamycin

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent / mercuric cyanide, Drierite / CH₂Cl₂ / 96 h / Heating

2: 1.) 1M aq. BaOH, 2.) H₂, Pd/C, AcOH / 1.) dioxane, 60 deg C, 6 h, 2.) dioxane, water

With calcium sulfate; barium dihydroxide; palladium on activated charcoal; hydrogen; mercury(II) cyanide; acetic acid; In dichloromethane;
DOI:10.1021/jo00334a042

Reference yield:

: 78763-86-7
3,2'-Di-N-(benzyloxycarbonyl)-3'-O-(tetrahydropyranyl)-2'',3'',5''-tri-O-acetyl-1,6:6',4'-N,O-carbonylthioribostamycin

: 78763-88-9
4''-Thioribostamycin

Guidance literature:: With barium dihydroxide; palladium on activated charcoal; hydrogen; acetic acid; Yield given. Multistep reaction; 1.) dioxane, 60 deg C, 6 h, 2.) dioxane, water;
DOI:10.1021/jo00334a042