5'-O-(tert-butyldimethylsilyl)-2',3'-didehydro-2',3'-dideoxy-2'-phenylthiouridine

Base Information

Chemical Name:5'-O-(tert-butyldimethylsilyl)-2',3'-didehydro-2',3'-dideoxy-2'-phenylthiouridine
CAS No.:475571-80-3
Molecular Formula:C₂₁H₂₈N₂O₄SSi
Molecular Weight:432.616
Hs Code.:

Synonyms:5'-O-(tert-butyldimethylsilyl)-2',3'-didehydro-2',3'-dideoxy-2'-phenylthiouridine

Suppliers and Price of 5'-O-(tert-butyldimethylsilyl)-2',3'-didehydro-2',3'-dideoxy-2'-phenylthiouridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5'-O-(tert-butyldimethylsilyl)-2',3'-didehydro-2',3'-dideoxy-2'-phenylthiouridine

Chemical Property:

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Technology Process of 5'-O-(tert-butyldimethylsilyl)-2',3'-didehydro-2',3'-dideoxy-2'-phenylthiouridine

There total 4 articles about 5'-O-(tert-butyldimethylsilyl)-2',3'-didehydro-2',3'-dideoxy-2'-phenylthiouridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 475571-79-0
5'-O-(tert-butyldimethylsilyl)-2'-deoxy-3'-O-methanesulfonyl-2'-phenylthiouridine

: 475571-80-3
5'-O-(tert-butyldimethylsilyl)-2',3'-didehydro-2',3'-dideoxy-2'-phenylthiouridine

Guidance literature:: With 2,6-dichloro-benzonitrile; In acetonitrile; for 2h; Heating;
DOI:10.1081/NCN-120006826

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 475571-80-3
5'-O-(tert-butyldimethylsilyl)-2',3'-didehydro-2',3'-dideoxy-2'-phenylthiouridine

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / pyridine / 15 h / 20 °C

2: 80 percent / pyridine / 12 h / 20 °C

3: 100 percent / DBN / acetonitrile / 2 h / Heating

With pyridine; 2,6-dichloro-benzonitrile; In acetonitrile;
DOI:10.1081/NCN-120006826

Reference yield:

: 83087-95-0
2'-deoxy-2'-phenylthiouridine

: 475571-80-3
5'-O-(tert-butyldimethylsilyl)-2',3'-didehydro-2',3'-dideoxy-2'-phenylthiouridine

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / pyridine / 15 h / 20 °C

2: 80 percent / pyridine / 12 h / 20 °C

3: 100 percent / DBN / acetonitrile / 2 h / Heating

With pyridine; 2,6-dichloro-benzonitrile; In acetonitrile;
DOI:10.1081/NCN-120006826