methyl 4-<<3-O-methyl-α-L-rhamnopyranosyl>oxy>-5-iodo-2,3-dimethoxy-6-methylbenzoate

Base Information

Chemical Name:methyl 4-<<3-O-methyl-α-L-rhamnopyranosyl>oxy>-5-iodo-2,3-dimethoxy-6-methylbenzoate
CAS No.:130851-56-8
Molecular Formula:C₁₈H₂₅IO₉
Molecular Weight:512.296
Hs Code.:

Synonyms:methyl 4-<<3-O-methyl-α-L-rhamnopyranosyl>oxy>-5-iodo-2,3-dimethoxy-6-methylbenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 4-<<3-O-methyl-α-L-rhamnopyranosyl>oxy>-5-iodo-2,3-dimethoxy-6-methylbenzoate

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Technology Process of methyl 4-<<3-O-methyl-α-L-rhamnopyranosyl>oxy>-5-iodo-2,3-dimethoxy-6-methylbenzoate

There total 19 articles about methyl 4-<<3-O-methyl-α-L-rhamnopyranosyl>oxy>-5-iodo-2,3-dimethoxy-6-methylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 131675-57-5
methyl 4-<<2,4-di-O-acetyl-3-O-methyl-α-L-rhamnopyranosyl>oxy>-5-iodo-2,3-dimethoxy-6-methylbenzoate

: 130851-56-8
methyl 4-<<3-O-methyl-α-L-rhamnopyranosyl>oxy>-5-iodo-2,3-dimethoxy-6-methylbenzoate

Guidance literature:: With potassium carbonate; In methanol; at 25 ℃; for 2h;
DOI:10.1039/c39900001275

Reference yield: 52.0%

: 130851-55-7
4-[(2S,3R,4R,5S,6S)-5-Acetoxy-3-(2,2-dimethyl-propionyloxy)-4-methoxy-6-methyl-tetrahydro-pyran-2-yloxy]-3-iodo-5,6-dimethoxy-2-methyl-benzoic acid methyl ester

: 130851-56-8
methyl 4-<<3-O-methyl-α-L-rhamnopyranosyl>oxy>-5-iodo-2,3-dimethoxy-6-methylbenzoate

Guidance literature:: With sodium methylate; In methanol; at 25 ℃; for 72h;
DOI:10.1016/S0040-4039(00)97556-7

Reference yield:

: 115592-74-0,115650-45-8,127761-05-1
4-Hydroxy-5-iod-2,3-dimethoxy-6-methyl-benzoesaeuremethylester

: 130851-56-8
methyl 4-<<3-O-methyl-α-L-rhamnopyranosyl>oxy>-5-iodo-2,3-dimethoxy-6-methylbenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / 4A molecular sieves, BF₃*OEt₂ / CH₂Cl₂ / 1 h / -65 - -50 °C

2: 93 percent / K₂CO₃ / tetrahydrofuran; methanol / 2.5 h / 25 °C

With 4 A molecular sieve; boron trifluoride diethyl etherate; potassium carbonate; In tetrahydrofuran; methanol; dichloromethane;