(1R,2R,6S,7S)-4-(2-{[1-Phenyl-meth-(E)-ylidene]-amino}-ethyl)-4-aza-tricyclo[5.2.1.0^2,6]dec-8-ene-3,5-dione

Base Information

• Chemical Name: (1R,2R,6S,7S)-4-(2-{[1-Phenyl-meth-(E)-ylidene]-amino}-ethyl)-4-aza-tricyclo[5.2.1.0^2,6]dec-8-ene-3,5-dione
• CAS No.: 406214-99-1
• Molecular Formula: C₁₈H₁₈N₂O₂
• Molecular Weight: 294.353

Synonyms:(1R,2R,6S,7S)-4-(2-{[1-Phenyl-meth-(E)-ylidene]-amino}-ethyl)-4-aza-tricyclo[5.2.1.0^2,6]dec-8-ene-3,5-dione

Chemical Property of (1R,2R,6S,7S)-4-(2-{[1-Phenyl-meth-(E)-ylidene]-amino}-ethyl)-4-aza-tricyclo[5.2.1.0^2,6]dec-8-ene-3,5-dione

Chemical Property:

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Technology Process of (1R,2R,6S,7S)-4-(2-{[1-Phenyl-meth-(E)-ylidene]-amino}-ethyl)-4-aza-tricyclo[5.2.1.0^2,6]dec-8-ene-3,5-dione

There total 3 articles about (1R,2R,6S,7S)-4-(2-{[1-Phenyl-meth-(E)-ylidene]-amino}-ethyl)-4-aza-tricyclo[5.2.1.0^2,6]dec-8-ene-3,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

benzaldehyde (100-52-7) + (1R,2R,6S,7S)-4-(2-Amino-ethyl)-4-aza-tricyclo[5.2.1.02,6]dec-8-ene-3,5-dione; compound with trifluoro-acetic acid → (1R,2R,6S,7S)-4-(2-{[1-Phenyl-meth-(E)-ylidene]-amino}-ethyl)-4-aza-tricyclo[5.2.1.02,6]dec-8-ene-3,5-dione (406214-99-1)

Guidance literature:

With magnesium sulfate; triethylamine; In dichloromethane;

Reference yield:

(1R,2R,6S,7S)-4-oxa-tricyclo[5.2.1.02,6]dec-8-ene-3,5-dione (2746-19-2) → (1R,2R,6S,7S)-4-(2-{[1-Phenyl-meth-(E)-ylidene]-amino}-ethyl)-4-aza-tricyclo[5.2.1.02,6]dec-8-ene-3,5-dione (406214-99-1)

Guidance literature:

Multi-step reaction with 3 steps

1: 92 percent / toluene / 64 h / Heating

2: 86 percent / CH₂Cl₂

3: 100 percent / Et₃N; MgSO₄ / CH₂Cl₂

With magnesium sulfate; triethylamine; In dichloromethane; toluene;

Reference yield:

(N-trityl-2-aminoethyl)-exo-norborn-5-ene-2,3-dicarboxylic imide → (1R,2R,6S,7S)-4-(2-{[1-Phenyl-meth-(E)-ylidene]-amino}-ethyl)-4-aza-tricyclo[5.2.1.02,6]dec-8-ene-3,5-dione (406214-99-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 86 percent / CH₂Cl₂

2: 100 percent / Et₃N; MgSO₄ / CH₂Cl₂

With magnesium sulfate; triethylamine; In dichloromethane;

upstream raw materials:

benzaldehyde

(1R,2R,6S,7S)-4-oxa-tricyclo[5.2.1.0^2,6]dec-8-ene-3,5-dione

Downstream raw materials:

Diphenyl-carbamic acid 2-acetylamino-9-({benzyl-[2-((1S,2S,6R,7R)-3,5-dioxo-4-aza-tricyclo[5.2.1.0^2,6]dec-8-en-4-yl)-ethyl]-carbamoyl}-methyl)-9H-purin-6-yl ester

2-(2-acetylamino-6-oxo-1,6-dihydro-purin-9-yl)-N-benzyl-N-[2-(3,5-dioxo-4-aza-tricyclo[5.2.1.0^2,6]dec-8-en-4-yl)-ethyl]-acetamide

[9-({benzyl-[2-(3,5-dioxo-4-aza-tricyclo[5.2.1.0^2,6]dec-8-en-4-yl)-ethyl]-carbamoyl}-methyl)-9H-purin-6-yl]-carbamic acid tert-butyl ester

2-(2-acetylamino-6-oxo-1,6-dihydro-purin-7-yl)-N-benzyl-N-[2-(3,5-dioxo-4-aza-tricyclo[5.2.1.0^2,6]dec-8-en-4-yl)-ethyl]-acetamide

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