3-(3-cyclopentyloxy-4-methoxyphenyl)-5-(trichloromethyl)-1,2,4-oxadiazole

Base Information

Chemical Name:3-(3-cyclopentyloxy-4-methoxyphenyl)-5-(trichloromethyl)-1,2,4-oxadiazole
CAS No.:1312793-89-7
Molecular Formula:C₁₅H₁₅Cl₃N₂O₃
Molecular Weight:377.655
Hs Code.:

Synonyms:3-(3-cyclopentyloxy-4-methoxyphenyl)-5-(trichloromethyl)-1,2,4-oxadiazole

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Chemical Property of 3-(3-cyclopentyloxy-4-methoxyphenyl)-5-(trichloromethyl)-1,2,4-oxadiazole

Chemical Property:

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Technology Process of 3-(3-cyclopentyloxy-4-methoxyphenyl)-5-(trichloromethyl)-1,2,4-oxadiazole

There total 3 articles about 3-(3-cyclopentyloxy-4-methoxyphenyl)-5-(trichloromethyl)-1,2,4-oxadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₅H₁₇Cl₃N₂O₄

: 1312793-89-7
3-(3-cyclopentyloxy-4-methoxyphenyl)-5-(trichloromethyl)-1,2,4-oxadiazole

Guidance literature:: In N,N-dimethyl-formamide; at 110 ℃; for 10h; Inert atmosphere;
DOI:10.1016/j.ejmech.2011.03.031

Reference yield:

: 874485-04-8
C₁₃H₁₈N₂O₃

: 1312793-89-7
3-(3-cyclopentyloxy-4-methoxyphenyl)-5-(trichloromethyl)-1,2,4-oxadiazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: dicyclohexyl-carbodiimide / N,N-dimethyl-formamide / 1 h / 0 °C / Inert atmosphere

1.2: 3.5 h / 0 - 30 °C / Inert atmosphere

2.1: N,N-dimethyl-formamide / 10 h / 110 °C / Inert atmosphere

With dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2011.03.031

Reference yield:

: 159783-16-1
3-(cyclopentyloxy)-4-methoxybenzonitrile

: 1312793-89-7
3-(3-cyclopentyloxy-4-methoxyphenyl)-5-(trichloromethyl)-1,2,4-oxadiazole

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydroxylamine hydrochloride; sodium carbonate / ethanol; water / 18 h / 0 °C / Reflux

2.1: dicyclohexyl-carbodiimide / N,N-dimethyl-formamide / 1 h / 0 °C / Inert atmosphere

2.2: 3.5 h / 0 - 30 °C / Inert atmosphere

3.1: N,N-dimethyl-formamide / 10 h / 110 °C / Inert atmosphere

With hydroxylamine hydrochloride; sodium carbonate; dicyclohexyl-carbodiimide; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2011.03.031