2-hydroxy-4-deuterio-anisole

Base Information

• Chemical Name: 2-hydroxy-4-deuterio-anisole
• CAS No.: 116467-77-7
• Molecular Formula: C₇H₈O₂
• Molecular Weight: 125.131

Synonyms:2-hydroxy-4-deuterio-anisole

Chemical Property of 2-hydroxy-4-deuterio-anisole

Chemical Property:

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Technology Process of 2-hydroxy-4-deuterio-anisole

There total 3 articles about 2-hydroxy-4-deuterio-anisole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(4-D)-Anisol (20938-43-6) → 2-hydroxy-4-deuterio-anisole (116467-77-7) + 4-methoxy-phenol (150-76-5) + C7H7(2)HO2

Guidance literature:

With ferrous perchlorate; copper(II) ion; dihydrogen peroxide; In water; at 25 ℃; for 0.5h; Product distribution; further oxidants and solvents;

DOI:10.1021/ja00230a032

Reference yield:

(4-D)-Anisol (20938-43-6) → 2-hydroxy-4-deuterio-anisole (116467-77-7) + C7H7(2)HO2 (80234-08-8) + 4-methoxy-phenol (150-76-5)

Guidance literature:

With 2-hydroperoxyhexafluoro-2-propanol; In 1,2-dichloro-ethane; at 80 ℃; for 16h; retention of deuterium in products;

DOI:10.1246/cl.1983.1707

Reference yield:

(4-D)-Anisol (20938-43-6) → 2-hydroxy-4-deuterio-anisole (116467-77-7) + C7H7(2)HO2 + C7H7(2)HO2 (80234-08-8) + 4-methoxy-phenol (150-76-5)

Guidance literature:

With O(³P) produced by microwave discharge; at -35 - 0 ℃; Product distribution; Mechanism; Distribution and deuterium content of products; triplet diradical intermediate; kinetic isotope effect; H-migration; temperature dependence;

DOI:10.1016/S0040-4039(00)71164-6

upstream raw materials:

(4-D)-Anisol

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