[RuClCp(PPh3)-μ-3,7-dimethyl-1,3,7-triaza-5-phosphabicyclo[3.3.1]nonane-1κP:2κ2N,N′-CoCl2]

Base Information

• Chemical Name: [RuClCp(PPh3)-μ-3,7-dimethyl-1,3,7-triaza-5-phosphabicyclo[3.3.1]nonane-1κP:2κ2N,N′-CoCl2]
• CAS No.: 1448257-06-4
• Molecular Formula: C₃₀H₃₆Cl₃CoN₃P₂Ru
• Molecular Weight: 767.006

Synonyms:[RuClCp(PPh3)-μ-3,7-dimethyl-1,3,7-triaza-5-phosphabicyclo[3.3.1]nonane-1κP:2κ2N,N′-CoCl2]

Chemical Property of [RuClCp(PPh3)-μ-3,7-dimethyl-1,3,7-triaza-5-phosphabicyclo[3.3.1]nonane-1κP:2κ2N,N′-CoCl2]

Chemical Property:

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Technology Process of [RuClCp(PPh3)-μ-3,7-dimethyl-1,3,7-triaza-5-phosphabicyclo[3.3.1]nonane-1κP:2κ2N,N′-CoCl2]

There total 1 articles about [RuClCp(PPh3)-μ-3,7-dimethyl-1,3,7-triaza-5-phosphabicyclo[3.3.1]nonane-1κP:2κ2N,N′-CoCl2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

[RuClCp(3,7-dimethyl-1,3,7-triaza-5-phosphabicyclo[3.3.1]nonane(+H))(PPh3)](OSO2CF3) + potassium tert-butylate (865-47-4) + cobalt(II) chloride (7646-79-9,14543-09-0,16413-89-1) → [RuClCp(PPh3)-μ-3,7-dimethyl-1,3,7-triaza-5-phosphabicyclo[3.3.1]nonane-1κP:2κ2N,N′-CoCl2] (1448257-06-4)

Guidance literature:

In ethanol; Inert atmosphere; Schlenk technique; Reflux;

DOI:10.1039/c3dt50829c

Reference yield:

[RuClCp(PPh3)-μ-3,7-dimethyl-1,3,7-triaza-5-phosphabicyclo[3.3.1]nonane-1κP:2κ2N,N′-CoCl2] (1448257-06-4) + silver trifluoromethanesulfonate (2923-28-6) → [RuClCp(3,7-dimethyl-1,3,7-triaza-5-phosphabicyclo[3.3.1]nonane)(PPh3)]*(OSO2CF3) (946088-18-2)

Guidance literature:

In water-d2; at 20 ℃;

DOI:10.1016/j.molcata.2015.10.004

upstream raw materials:

potassium tert-butylate

cobalt(II) chloride

Downstream raw materials:

[RuClCp(3,7-dimethyl-1,3,7-triaza-5-phosphabicyclo[3.3.1]nonane)(PPh₃)]*(OSO₂CF₃)

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