C₁₁H₁₅IO₂

Base Information

Chemical Name:C₁₁H₁₅IO₂
CAS No.:1445569-37-8
Molecular Formula:C₁₁H₁₅IO₂
Molecular Weight:306.143
Hs Code.:

C<sub>11</sub>H<sub>15</sub>IO<sub>2</sub>

Synonyms:C₁₁H₁₅IO₂

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Chemical Property of C₁₁H₁₅IO₂

Chemical Property:

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Technology Process of C₁₁H₁₅IO₂

There total 1 articles about C₁₁H₁₅IO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 71720-27-9
3-Isopropyl-veratrol

: 1445569-37-8
C₁₁H₁₅IO₂

Guidance literature:: 3-Isopropyl-veratrol; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In diethyl ether; hexane; at 0 - 20 ℃; Inert atmosphere;

With iodine; In diethyl ether; hexane; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol401543b

Reference yield: 100.0%

: 1445569-37-8
C₁₁H₁₅IO₂

: 1066-54-2
trimethylsilylacetylene

: 1445569-41-4
(4-isopropyl-2,3-dimethoxyphenyl)ethynyltrimethylsilane

Guidance literature:: C₁₁H₁₅IO₂; With copper(l) iodide; diisopropylamine; triphenylphosphine; palladium dichloride; In tetrahydrofuran; at 20 ℃; for 0.5h; Inert atmosphere;

trimethylsilylacetylene; In tetrahydrofuran; for 12h; Reflux; Inert atmosphere;
DOI:10.1021/ol401543b

Reference yield:

: 1445569-37-8
C₁₁H₁₅IO₂

: C₂₃H₃₄O₄

Guidance literature:: Multi-step reaction with 7 steps

1.1: palladium dichloride; triphenylphosphine; copper(l) iodide; diisopropylamine / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

1.2: 12 h / Reflux; Inert atmosphere

2.1: potassium carbonate / methanol / 1 h / 20 °C / Inert atmosphere

3.1: diethylzinc / hexane; toluene / 4 h / Reflux; Inert atmosphere

3.2: 1 h / 20 °C / Inert atmosphere

3.3: 12 h / 20 °C / Inert atmosphere

4.1: sodium bis(2-methoxyethoxy)aluminium dihydride / toluene; diethyl ether / 0 - 20 °C / Inert atmosphere

4.2: 2 h / -78 °C / Inert atmosphere

5.1: 2,6-dimethylpyridine / dichloromethane / 4 h / 0 °C / Inert atmosphere

6.1: triethylamine; bis-triphenylphosphine-palladium(II) chloride / water; N,N-dimethyl-formamide / 30 h / 80 °C

7.1: tetrabutyl ammonium fluoride / benzene-d6 / 70 °C

With 2,6-dimethylpyridine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrabutyl ammonium fluoride; diethylzinc; potassium carbonate; triethylamine; diisopropylamine; triphenylphosphine; sodium bis(2-methoxyethoxy)aluminium dihydride; palladium dichloride; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; benzene-d6; water; N,N-dimethyl-formamide; toluene; 1.2: |Sonogashira Cross-Coupling / 6.1: |Heck Reaction;
DOI:10.1021/ol401543b