C-Phenyl-C-((3R,5S,8aR)-3-phenyl-hexahydro-oxazolo[3,2-a]pyridin-5-yl)-methyleneamine

Base Information

Chemical Name:C-Phenyl-C-((3R,5S,8aR)-3-phenyl-hexahydro-oxazolo[3,2-a]pyridin-5-yl)-methyleneamine
CAS No.:119020-93-8
Molecular Formula:C₂₀H₂₂N₂O
Molecular Weight:306.407
Hs Code.:

Synonyms:C-Phenyl-C-((3R,5S,8aR)-3-phenyl-hexahydro-oxazolo[3,2-a]pyridin-5-yl)-methyleneamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C-Phenyl-C-((3R,5S,8aR)-3-phenyl-hexahydro-oxazolo[3,2-a]pyridin-5-yl)-methyleneamine

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Technology Process of C-Phenyl-C-((3R,5S,8aR)-3-phenyl-hexahydro-oxazolo[3,2-a]pyridin-5-yl)-methyleneamine

There total 1 articles about C-Phenyl-C-((3R,5S,8aR)-3-phenyl-hexahydro-oxazolo[3,2-a]pyridin-5-yl)-methyleneamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 88056-92-2
(-)-2-cyano-6-phenyloxazolopiperidine

: 591-51-5
phenyllithium

: 119020-93-8
C-Phenyl-C-((3R,5S,8aR)-3-phenyl-hexahydro-oxazolo[3,2-a]pyridin-5-yl)-methyleneamine

Guidance literature:: In diethyl ether; at -70 ℃; for 1.5h;

Reference yield: 86.0%

: 119020-93-8
C-Phenyl-C-((3R,5S,8aR)-3-phenyl-hexahydro-oxazolo[3,2-a]pyridin-5-yl)-methyleneamine

: 119020-94-9,119069-10-2
Phenyl-((3R,8aR)-3-phenyl-hexahydro-oxazolo[3,2-a]pyridin-5-yl)-methanone

Guidance literature:: With hydrogenchloride; In diethyl ether; water; for 1h; Ambient temperature;

Reference yield:

: 119020-93-8
C-Phenyl-C-((3R,5S,8aR)-3-phenyl-hexahydro-oxazolo[3,2-a]pyridin-5-yl)-methyleneamine

: 5583-31-3
(αR,2S)-phenyl 2-piperidyl methanol

Guidance literature:: Multi-step reaction with 4 steps

1: 86 percent / 2N HCl / diethyl ether; H₂O / 1 h / Ambient temperature

2: 75 percent / hydrogen / PtO₂ / methanol; HCl / 12 h / Ambient temperature

3: 64 percent / LiAlH₄, AlCl₃ / diethyl ether / 3 h / -30 - -10 °C

4: hydrogen / Pd(OH)2 / methanol

With hydrogenchloride; lithium aluminium tetrahydride; aluminium trichloride; hydrogen; platinum(IV) oxide; palladium dihydroxide; In hydrogenchloride; methanol; diethyl ether; water;