N-(4,4'-diamino-biphenyl-2-ylmethyl)-3-{(2-tritylsulfanyl-ethyl)-[(2-tritylsulfanyl-ethylcarbamoyl)-methyl]-amino}-propionamide

Base Information

Chemical Name:N-(4,4'-diamino-biphenyl-2-ylmethyl)-3-{(2-tritylsulfanyl-ethyl)-[(2-tritylsulfanyl-ethylcarbamoyl)-methyl]-amino}-propionamide
CAS No.:199273-21-7
Molecular Formula:C₆₀H₅₉N₅O₂S₂
Molecular Weight:946.293
Hs Code.:

<i>N</i>-(4,4'-diamino-biphenyl-2-ylmethyl)-3-{(2-tritylsulfanyl-ethyl)-[(2-tritylsulfanyl-ethylcarbamoyl)-methyl]-amino}-propionamide

Synonyms:N-(4,4'-diamino-biphenyl-2-ylmethyl)-3-{(2-tritylsulfanyl-ethyl)-[(2-tritylsulfanyl-ethylcarbamoyl)-methyl]-amino}-propionamide

Suppliers and Price of N-(4,4'-diamino-biphenyl-2-ylmethyl)-3-{(2-tritylsulfanyl-ethyl)-[(2-tritylsulfanyl-ethylcarbamoyl)-methyl]-amino}-propionamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of N-(4,4'-diamino-biphenyl-2-ylmethyl)-3-{(2-tritylsulfanyl-ethyl)-[(2-tritylsulfanyl-ethylcarbamoyl)-methyl]-amino}-propionamide

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Hazard Codes:

MSDS Files:

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Technology Process of N-(4,4'-diamino-biphenyl-2-ylmethyl)-3-{(2-tritylsulfanyl-ethyl)-[(2-tritylsulfanyl-ethylcarbamoyl)-methyl]-amino}-propionamide

There total 8 articles about N-(4,4'-diamino-biphenyl-2-ylmethyl)-3-{(2-tritylsulfanyl-ethyl)-[(2-tritylsulfanyl-ethylcarbamoyl)-methyl]-amino}-propionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 51787-75-8
4,4'-dinitro-2-biphenylamine

: 199273-21-7
N-(4,4'-diamino-biphenyl-2-ylmethyl)-3-{(2-tritylsulfanyl-ethyl)-[(2-tritylsulfanyl-ethylcarbamoyl)-methyl]-amino}-propionamide

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) H₂SO₄, NaNO₂, H₃PO₄, 2.) aq. KI / 1.) from 5 to 10 deg C, 2.) 70 deg C

2: 90 percent / dimethylsulfoxide / 2 h / 180 °C

3: H₂ / 10 percent Pd/C / methanol / 24 h / 2844.31 Torr

4: LiAlH₄ / tetrahydrofuran / 8 h / Heating

5: tetrahydrofuran / 2 h / Ambient temperature

With lithium aluminium tetrahydride; phosphoric acid; sulfuric acid; hydrogen; potassium iodide; sodium nitrite; palladium on activated charcoal; In tetrahydrofuran; methanol; dimethyl sulfoxide;
DOI:10.1021/jm990103w

Reference yield:

: 146901-97-5
2-iodo-4,4'-dinitrobiphenyl

: 199273-21-7
N-(4,4'-diamino-biphenyl-2-ylmethyl)-3-{(2-tritylsulfanyl-ethyl)-[(2-tritylsulfanyl-ethylcarbamoyl)-methyl]-amino}-propionamide

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / dimethylsulfoxide / 2 h / 180 °C

2: H₂ / 10 percent Pd/C / methanol / 24 h / 2844.31 Torr

3: LiAlH₄ / tetrahydrofuran / 8 h / Heating

4: tetrahydrofuran / 2 h / Ambient temperature

With lithium aluminium tetrahydride; hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol; dimethyl sulfoxide;
DOI:10.1021/jm990103w

Reference yield:

: 199273-18-2
2-cyano-4,4'-dinitrobiphenyl

: 199273-21-7
N-(4,4'-diamino-biphenyl-2-ylmethyl)-3-{(2-tritylsulfanyl-ethyl)-[(2-tritylsulfanyl-ethylcarbamoyl)-methyl]-amino}-propionamide

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / 10 percent Pd/C / methanol / 24 h / 2844.31 Torr

2: LiAlH₄ / tetrahydrofuran / 8 h / Heating

3: tetrahydrofuran / 2 h / Ambient temperature

With lithium aluminium tetrahydride; hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol;
DOI:10.1021/jm990103w